N-[benzyloxycarbonyl]-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanine-N-methyl-N-phenylamide

Base Information

Chemical Name:N-[benzyloxycarbonyl]-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanine-N-methyl-N-phenylamide
CAS No.:1312775-20-4
Molecular Formula:C₃₅H₅₀N₆O₇
Molecular Weight:666.818
Hs Code.:

Synonyms:N-[benzyloxycarbonyl]-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanine-N-methyl-N-phenylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[benzyloxycarbonyl]-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanine-N-methyl-N-phenylamide

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Technology Process of N-[benzyloxycarbonyl]-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanine-N-methyl-N-phenylamide

There total 8 articles about N-[benzyloxycarbonyl]-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanine-N-methyl-N-phenylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 4512-42-9
N-[benzyloxycarbonyl]-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanine

: 75755-40-7
2,2-dimethyl-3-(N-methyl-N-phenylamino)-2H-azirine

: 1312775-20-4
N-[benzyloxycarbonyl]-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanine-N-methyl-N-phenylamide

Guidance literature:: In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1002/hlca.201100116

Reference yield:

: 15030-72-5
Z-Aib-OH

: 1312775-20-4
N-[benzyloxycarbonyl]-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanine-N-methyl-N-phenylamide

Guidance literature:: Multi-step reaction with 7 steps

1: diethyl ether / 0 - 20 °C

2: hydrogenchloride; water / tetrahydrofuran / 20 °C

3: tetrahydrofuran / 4.16 h / 0 - 20 °C

4: hydrogenchloride; water / tetrahydrofuran / 2 h / 20 °C

5: N,N-dimethyl-formamide / 4.16 h / 0 - 20 °C

6: hydrogenchloride; water / tetrahydrofuran / 2.5 h / 20 °C

7: N,N-dimethyl-formamide / 0 - 20 °C

With hydrogenchloride; water; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1002/hlca.201100116

Reference yield:

: 111492-19-4
2-<2-(Benzyloxycarboxamido)-2-methylpropionamido>-N,N,2-trimethylpropionamid

: 1312775-20-4
N-[benzyloxycarbonyl]-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanyl-2-methylalanine-N-methyl-N-phenylamide

Guidance literature:: Multi-step reaction with 6 steps

1: hydrogenchloride; water / tetrahydrofuran / 20 °C

2: tetrahydrofuran / 4.16 h / 0 - 20 °C

3: hydrogenchloride; water / tetrahydrofuran / 2 h / 20 °C

4: N,N-dimethyl-formamide / 4.16 h / 0 - 20 °C

5: hydrogenchloride; water / tetrahydrofuran / 2.5 h / 20 °C

6: N,N-dimethyl-formamide / 0 - 20 °C

With hydrogenchloride; water; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/hlca.201100116