piperidine-1-sulfonic acid (4-{2-[5(R)-(3-chloro-phenyl)-2-oxo-oxazolidin-3-yl]-2-methyl-propyl}-phenyl)-amide

Base Information

• Chemical Name: piperidine-1-sulfonic acid (4-{2-[5(R)-(3-chloro-phenyl)-2-oxo-oxazolidin-3-yl]-2-methyl-propyl}-phenyl)-amide
• CAS No.: 454219-01-3
• Molecular Formula: C₂₄H₃₀ClN₃O₄S
• Molecular Weight: 492.039

Synonyms:piperidine-1-sulfonic acid (4-{2-[5(R)-(3-chloro-phenyl)-2-oxo-oxazolidin-3-yl]-2-methyl-propyl}-phenyl)-amide

Chemical Property of piperidine-1-sulfonic acid (4-{2-[5(R)-(3-chloro-phenyl)-2-oxo-oxazolidin-3-yl]-2-methyl-propyl}-phenyl)-amide

Chemical Property:

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Technology Process of piperidine-1-sulfonic acid (4-{2-[5(R)-(3-chloro-phenyl)-2-oxo-oxazolidin-3-yl]-2-methyl-propyl}-phenyl)-amide

There total 2 articles about piperidine-1-sulfonic acid (4-{2-[5(R)-(3-chloro-phenyl)-2-oxo-oxazolidin-3-yl]-2-methyl-propyl}-phenyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3(R)-[2-(4-amino-phenyl)-1,1-dimethyl-ethyl]-5-(3-chloro-phenyl)-oxazolidin-2-one + piperidylsulphamoyl chloride (89316-33-6) → piperidine-1-sulfonic acid (4-{2-[5(R)-(3-chloro-phenyl)-2-oxo-oxazolidin-3-yl]-2-methyl-propyl}-phenyl)-amide (454219-01-3)

Guidance literature:

With triethylamine; In ethyl acetate; 1,2-dichloro-ethane;

Reference yield:

3(R)-[2-(4-amino-phenyl)-1,1-dimethyl-ethyl]-5-(3-chloro-phenyl)-oxazolidin-2-one + 1-piperidinesulfonyl chloride (35856-62-3) → piperidine-1-sulfonic acid (4-{2-[5(R)-(3-chloro-phenyl)-2-oxo-oxazolidin-3-yl]-2-methyl-propyl}-phenyl)-amide (454219-01-3)

Guidance literature:

With triethylamine; In 1,2-dichloro-ethane; at 0 - 65 ℃; for 22.25h;

Reference yield:

acetate + piperidine-1-sulfonic acid (4-{2-[5(R)-(3-chloro-phenyl)-2-oxo-oxazolidin-3-yl]-2-methyl-propyl}-phenyl)-amide (454219-01-3) → N-[4-[2-[[(2R)-2-(3-chlorophenyl)-2-hydroxyethyl]amino]-2-methylpropyl]phenyl]-1-piperidinesulfonamide, dihydrochloride

Guidance literature:

With hydrogenchloride; potassium hydroxide; In diethyl ether; ethanol; dimethyl sulfoxide;

upstream raw materials:

1-piperidinesulfonyl chloride

piperidylsulphamoyl chloride

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