C₄₆H₅₃NO₃

Base Information

Chemical Name:C₄₆H₅₃NO₃
CAS No.:1404213-32-6
Molecular Formula:C₄₆H₅₃NO₃
Molecular Weight:667.932
Hs Code.:

C<sub>46</sub>H<sub>53</sub>NO<sub>3</sub>

Synonyms:C₄₆H₅₃NO₃

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Chemical Property of C₄₆H₅₃NO₃

Chemical Property:

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Technology Process of C₄₆H₅₃NO₃

There total 8 articles about C₄₆H₅₃NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1404213-31-5
C₅₂H₆₉NO₃Si₂

: 1404213-32-6
C₄₆H₅₃NO₃

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.5h;
DOI:10.1002/ejoc.201200655

Reference yield:

: 149505-94-2
tert-butyl (4-hydroxybenzyl)carbamate

: 1404213-32-6
C₄₆H₅₃NO₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium chlorite; sodium iodide / methanol; water

1.2: 20 °C

2.1: potassium carbonate / acetone / Inert atmosphere; Reflux

3.1: trifluoroacetic acid / dichloromethane / 2 h

3.2: 20 °C / Inert atmosphere

4.1: boron tribromide / dichloromethane / -78 - 20 °C / Inert atmosphere

5.1: sodium iodide; potassium carbonate / acetone / Reflux

6.1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 20 °C / Inert atmosphere

7.1: potassium hydroxide / methanol; tetrahydrofuran / 1 h

7.2: Inert atmosphere

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; sodium chlorite; copper(l) iodide; tetrabutyl ammonium fluoride; boron tribromide; potassium carbonate; triethylamine; trifluoroacetic acid; sodium iodide; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; acetone; 6.1: |Sonogashira Cross-Coupling / 7.2: |Sonogashira Cross-Coupling;
DOI:10.1002/ejoc.201200655

Reference yield:

: 1404213-29-1
C₂₂H₃₅I₂NO₃

: 1404213-32-6
C₄₆H₅₃NO₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 20 °C / Inert atmosphere

2.1: potassium hydroxide / methanol; tetrahydrofuran / 1 h

2.2: Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine; potassium hydroxide; In tetrahydrofuran; methanol; 1.1: |Sonogashira Cross-Coupling / 2.2: |Sonogashira Cross-Coupling;
DOI:10.1002/ejoc.201200655