18-[2-(benzyloxy)ethyl]-2,34-dimethyl-6,30-bis(4-methylpentyl)-10,26-bis[8-methyl-4-(4-methylpentyl)nonyl]-14,22-bis{12-methyl-8-(4-methylpentyl)-4-[8-methyl-4-(4-methylpentyl)nonyl]tridecyl}pentatriacontane-14,22-diol

Base Information

• Chemical Name: 18-[2-(benzyloxy)ethyl]-2,34-dimethyl-6,30-bis(4-methylpentyl)-10,26-bis[8-methyl-4-(4-methylpentyl)nonyl]-14,22-bis{12-methyl-8-(4-methylpentyl)-4-[8-methyl-4-(4-methylpentyl)nonyl]tridecyl}pentatriacontane-14,22-diol
• CAS No.: 1356140-48-1
• Molecular Formula: C₁₆₂H₃₁₈O₃
• Molecular Weight: 2314.31

Synonyms:18-[2-(benzyloxy)ethyl]-2,34-dimethyl-6,30-bis(4-methylpentyl)-10,26-bis[8-methyl-4-(4-methylpentyl)nonyl]-14,22-bis{12-methyl-8-(4-methylpentyl)-4-[8-methyl-4-(4-methylpentyl)nonyl]tridecyl}pentatriacontane-14,22-diol

Chemical Property of 18-[2-(benzyloxy)ethyl]-2,34-dimethyl-6,30-bis(4-methylpentyl)-10,26-bis[8-methyl-4-(4-methylpentyl)nonyl]-14,22-bis{12-methyl-8-(4-methylpentyl)-4-[8-methyl-4-(4-methylpentyl)nonyl]tridecyl}pentatriacontane-14,22-diol

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Technology Process of 18-[2-(benzyloxy)ethyl]-2,34-dimethyl-6,30-bis(4-methylpentyl)-10,26-bis[8-methyl-4-(4-methylpentyl)nonyl]-14,22-bis{12-methyl-8-(4-methylpentyl)-4-[8-methyl-4-(4-methylpentyl)nonyl]tridecyl}pentatriacontane-14,22-diol

There total 2 articles about 18-[2-(benzyloxy)ethyl]-2,34-dimethyl-6,30-bis(4-methylpentyl)-10,26-bis[8-methyl-4-(4-methylpentyl)nonyl]-14,22-bis{12-methyl-8-(4-methylpentyl)-4-[8-methyl-4-(4-methylpentyl)nonyl]tridecyl}pentatriacontane-14,22-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

1-iodo-12-methyl-8-(4-methylpentyl)-4-[8-methyl-4-(4-methylpentyl)nonyl]tridecane (1356140-47-0) + ethyl 5-[2-(benzyloxy)ethyl]-9-hydroxy-21-methyl-17-(4-methylpentyl)-13-[8-methyl-4-(4-methylpentyl)nonyl]-9-{12-methyl-8-(4-methylpentyl)-4-[8-methyl-4-(4-methylpentyl)nonyl]tridecyl}docosanoate (1356140-49-2) → 18-[2-(benzyloxy)ethyl]-2,34-dimethyl-6,30-bis(4-methylpentyl)-10,26-bis[8-methyl-4-(4-methylpentyl)nonyl]-14,22-bis{12-methyl-8-(4-methylpentyl)-4-[8-methyl-4-(4-methylpentyl)nonyl]tridecyl}pentatriacontane-14,22-diol (1356140-48-1)

Guidance literature:

With samarium diiodide; nickel(I) iodide; In tetrahydrofuran; at 20 ℃; for 2.33333h; Inert atmosphere;

DOI:10.1002/asia.201100480

Reference yield: 51.0%

diethyl 5-[2-(benzyloxy)ethyl]nonanedioate + 1-iodo-12-methyl-8-(4-methylpentyl)-4-[8-methyl-4-(4-methylpentyl)nonyl]tridecane (1356140-47-0) → ethyl 5-[2-(benzyloxy)ethyl]-9-hydroxy-21-methyl-17-(4-methylpentyl)-13-[8-methyl-4-(4-methylpentyl)nonyl]-9-{12-methyl-8-(4-methylpentyl)-4-[8-methyl-4-(4-methylpentyl)nonyl]tridecyl}docosanoate (1356140-49-2) + 18-[2-(benzyloxy)ethyl]-2,34-dimethyl-6,30-bis(4-methylpentyl)-10,26-bis[8-methyl-4-(4-methylpentyl)nonyl]-14,22-bis{12-methyl-8-(4-methylpentyl)-4-[8-methyl-4-(4-methylpentyl)nonyl]tridecyl}pentatriacontane-14,22-diol (1356140-48-1)

Guidance literature:

With samarium diiodide; nickel(I) iodide; In tetrahydrofuran; at 20 ℃; for 2.33333h; Inert atmosphere;

DOI:10.1002/asia.201100480

upstream raw materials:

1-iodo-12-methyl-8-(4-methylpentyl)-4-[8-methyl-4-(4-methylpentyl)nonyl]tridecane

ethyl 5-[2-(benzyloxy)ethyl]-9-hydroxy-21-methyl-17-(4-methylpentyl)-13-[8-methyl-4-(4-methylpentyl)nonyl]-9-{12-methyl-8-(4-methylpentyl)-4-[8-methyl-4-(4-methylpentyl)nonyl]tridecyl}docosanoate

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