1-iodo-12-methyl-8-(4-methylpentyl)-4-[8-methyl-4-(4-methylpentyl)nonyl]tridecane

Base Information

Chemical Name:1-iodo-12-methyl-8-(4-methylpentyl)-4-[8-methyl-4-(4-methylpentyl)nonyl]tridecane
CAS No.:1356140-47-0
Molecular Formula:C₃₆H₇₃I
Molecular Weight:632.88
Hs Code.:

Synonyms:1-iodo-12-methyl-8-(4-methylpentyl)-4-[8-methyl-4-(4-methylpentyl)nonyl]tridecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-iodo-12-methyl-8-(4-methylpentyl)-4-[8-methyl-4-(4-methylpentyl)nonyl]tridecane

Chemical Property:

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Technology Process of 1-iodo-12-methyl-8-(4-methylpentyl)-4-[8-methyl-4-(4-methylpentyl)nonyl]tridecane

There total 11 articles about 1-iodo-12-methyl-8-(4-methylpentyl)-4-[8-methyl-4-(4-methylpentyl)nonyl]tridecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374442-63-3
C₃₆H₇₄O

: 1356140-47-0
1-iodo-12-methyl-8-(4-methylpentyl)-4-[8-methyl-4-(4-methylpentyl)nonyl]tridecane

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In dichloromethane; at 20 ℃; for 6h;
DOI:10.1002/asia.201100480

Reference yield:

: 1187663-04-2
C₁₉H₃₂O₄

: 1356140-47-0
1-iodo-12-methyl-8-(4-methylpentyl)-4-[8-methyl-4-(4-methylpentyl)nonyl]tridecane

Guidance literature:: Multi-step reaction with 5 steps

1.1: Jones reagent / acetone

2.1: sulfuric acid / 12 h / Reflux

2.2: 6 h / 20 °C / 760.05 Torr

3.1: iodine; magnesium / diethyl ether / 2 h / Inert atmosphere; Reflux

3.2: 5 h / Inert atmosphere; Reflux

4.1: triethylsilane; trifluoroacetic acid / dichloromethane / 12 h / 20 °C

4.2: 6 h / 20 °C / 760.05 Torr

5.1: 1H-imidazole; iodine; triphenylphosphine / dichloromethane / 6 h / 20 °C

With 1H-imidazole; triethylsilane; Jones reagent; sulfuric acid; iodine; magnesium; triphenylphosphine; trifluoroacetic acid; In diethyl ether; dichloromethane; acetone; 1.1: Jones oxidation;
DOI:10.1002/asia.201100480

Reference yield:

: C₁₉H₂₈O₆

: 1356140-47-0
1-iodo-12-methyl-8-(4-methylpentyl)-4-[8-methyl-4-(4-methylpentyl)nonyl]tridecane

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid / 12 h / Reflux

1.2: 6 h / 20 °C / 760.05 Torr

2.1: iodine; magnesium / diethyl ether / 2 h / Inert atmosphere; Reflux

2.2: 5 h / Inert atmosphere; Reflux

3.1: triethylsilane; trifluoroacetic acid / dichloromethane / 12 h / 20 °C

3.2: 6 h / 20 °C / 760.05 Torr

4.1: 1H-imidazole; iodine; triphenylphosphine / dichloromethane / 6 h / 20 °C

With 1H-imidazole; triethylsilane; sulfuric acid; iodine; magnesium; triphenylphosphine; trifluoroacetic acid; In diethyl ether; dichloromethane;
DOI:10.1002/asia.201100480