1L-7-O-Benzyl-1-desoxy-1-C-(hydroxymethyl)-2,3:4,5-di-O-isopropyliden-6-O-methyl-myo-inosit

Base Information

Chemical Name:1L-7-O-Benzyl-1-desoxy-1-C-(hydroxymethyl)-2,3:4,5-di-O-isopropyliden-6-O-methyl-myo-inosit
CAS No.:97119-62-5
Molecular Formula:C₂₁H₃₀O₆
Molecular Weight:380.45
Hs Code.:

1L-7-O-<D2>Benzyl-1-desoxy-1-C-(hydroxymethyl)-2,3:4,5-di-O-isopropyliden-6-O-methyl-myo-inosit

Synonyms:1L-7-O-Benzyl-1-desoxy-1-C-(hydroxymethyl)-2,3:4,5-di-O-isopropyliden-6-O-methyl-myo-inosit

Suppliers and Price of 1L-7-O-Benzyl-1-desoxy-1-C-(hydroxymethyl)-2,3:4,5-di-O-isopropyliden-6-O-methyl-myo-inosit

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1L-7-O-Benzyl-1-desoxy-1-C-(hydroxymethyl)-2,3:4,5-di-O-isopropyliden-6-O-methyl-myo-inosit

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1L-7-O-Benzyl-1-desoxy-1-C-(hydroxymethyl)-2,3:4,5-di-O-isopropyliden-6-O-methyl-myo-inosit

There total 1 articles about 1L-7-O-Benzyl-1-desoxy-1-C-(hydroxymethyl)-2,3:4,5-di-O-isopropyliden-6-O-methyl-myo-inosit which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 51271-29-5
[1',1'-2H₂]benzyl bromide

: 86845-47-8,86853-27-2
1L-1-Desoxy-1-C-hydroxymethyl-2,3:4,5-di-O-isopropyliden-6-O-methyl-myo-inosit

: 97119-62-5
1L-7-O-Benzyl-1-desoxy-1-C-(hydroxymethyl)-2,3:4,5-di-O-isopropyliden-6-O-methyl-myo-inosit

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; 1) 2 h, 0 deg C, 2) 5 h, room temp.;

Reference yield: 81.0%

: 97119-62-5
1L-7-O-Benzyl-1-desoxy-1-C-(hydroxymethyl)-2,3:4,5-di-O-isopropyliden-6-O-methyl-myo-inosit

: 97136-90-8
1L-7-O-Benzyl-1-desoxy-1-C-(hydroxymethyl)-2,3-O-isopropyliden-6-O-methyl-myo-inosit

Guidance literature:: With acetic acid; at 30 ℃;

Reference yield:

: 97119-62-5
1L-7-O-Benzyl-1-desoxy-1-C-(hydroxymethyl)-2,3:4,5-di-O-isopropyliden-6-O-methyl-myo-inosit

: 97119-14-7
3-O-Acetyl-4-<1D-(1N,2,4/3,5,6)-<6-O-acetyl-2,3,4,6-tetrahydroxy-5-C-(hydroxymethyl)-4-O-methylcyclohexyl>amino>-1,6-anhydro-4-desoxy-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 9 steps

1: 81 percent / 98percent acetic acid / 30 °C

2: 91 percent / 1) NaH / dimethylformamide / 1) 2 h, 0 deg C, 2) 5 h, room temp.

3: 91 percent / acetic acid / tetrahydrofuran; H₂O / 60 °C

4: 89 percent / pyridine / CH₂Cl₂ / -40 °C

5: 69 percent / NaN₃ / hexamethylphosphoric acid triamide / 30 °C

6: 86 percent / 4percent NiCl₂-solution, NaBH₄ / ethanol

7: butan-1-ol / 30 h / 110 °C

8: pyridine / 40 °C

9: 94 percent / H₂ / 10percent Pd/C / methanol / 2 h / 6000.5 Torr

With pyridine; sodium tetrahydroborate; sodium azide; hydrogen; sodium hydride; acetic acid; nickel dichloride; palladium on activated charcoal; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; dichloromethane; water; N,N-dimethyl-formamide; butan-1-ol;