2-[2-chloro-4-(4-chlorophenoxy)phenyl]-1-(1,2,4-triazol-1-yl)but-3-en-2-ol

Base Information

Chemical Name:2-[2-chloro-4-(4-chlorophenoxy)phenyl]-1-(1,2,4-triazol-1-yl)but-3-en-2-ol
CAS No.:1419875-43-6
Molecular Formula:C₁₈H₁₅Cl₂N₃O₂
Molecular Weight:376.242
Hs Code.:

Synonyms:2-[2-chloro-4-(4-chlorophenoxy)phenyl]-1-(1,2,4-triazol-1-yl)but-3-en-2-ol

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Chemical Property of 2-[2-chloro-4-(4-chlorophenoxy)phenyl]-1-(1,2,4-triazol-1-yl)but-3-en-2-ol

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Technology Process of 2-[2-chloro-4-(4-chlorophenoxy)phenyl]-1-(1,2,4-triazol-1-yl)but-3-en-2-ol

There total 3 articles about 2-[2-chloro-4-(4-chlorophenoxy)phenyl]-1-(1,2,4-triazol-1-yl)but-3-en-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 136815-80-0
1-[2-chloro-4-(4-chloro-phenoxy)-phenyl]-2-[1,2,4]triazol-1-yl-ethanone

: 3536-96-7
vinylmagnesium chloride

: 1419875-43-6
2-[2-chloro-4-(4-chlorophenoxy)phenyl]-1-(1,2,4-triazol-1-yl)but-3-en-2-ol

Guidance literature:: 1-[2-chloro-4-(4-chloro-phenoxy)-phenyl]-2-[1,2,4]triazol-1-yl-ethanone; With magnesiumbromide etherate; In dichloromethane; at 20 ℃; for 1h;

vinylmagnesium chloride; In diethyl ether; dichloromethane; at -15 ℃; for 2h;

Reference yield:

: 906005-51-4
2-bromo-1-(2-chloro-4-(4-chlorophenoxy)phenyl)ethanone

: 1419875-43-6
2-[2-chloro-4-(4-chlorophenoxy)phenyl]-1-(1,2,4-triazol-1-yl)but-3-en-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h

1.2: 2.5 h

2.1: magnesiumbromide etherate / dichloromethane / 1 h / 20 °C

2.2: 2 h / -15 °C

With magnesiumbromide etherate; sodium hydride; In tetrahydrofuran; dichloromethane;

Reference yield:

: 119851-28-4
1-(2-chloro-4-(4-chlorophenoxy)phenyl)-ethan-1-one

: 1419875-43-6
2-[2-chloro-4-(4-chlorophenoxy)phenyl]-1-(1,2,4-triazol-1-yl)but-3-en-2-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: bromine; acetic acid / tert-butyl methyl ether / 1 h / 20 °C

2.1: sodium hydride / tetrahydrofuran / 0.5 h

2.2: 2.5 h

3.1: magnesiumbromide etherate / dichloromethane / 1 h / 20 °C

3.2: 2 h / -15 °C

With magnesiumbromide etherate; bromine; sodium hydride; acetic acid; In tetrahydrofuran; dichloromethane; tert-butyl methyl ether;