1-[2-{2-(2-aminoethoxy)ethoxy}ethyl] β-lactoside

Base Information

• Chemical Name: 1-[2-{2-(2-aminoethoxy)ethoxy}ethyl] β-lactoside
• CAS No.: 879004-80-5
• Molecular Formula: C₁₈H₃₅NO₁₃
• Molecular Weight: 473.475
• Mol file: 879004-80-5.mol

Synonyms:1-[2-{2-(2-aminoethoxy)ethoxy}ethyl] β-lactoside

Chemical Property of 1-[2-{2-(2-aminoethoxy)ethoxy}ethyl] β-lactoside

Chemical Property:

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Technology Process of 1-[2-{2-(2-aminoethoxy)ethoxy}ethyl] β-lactoside

There total 1 articles about 1-[2-{2-(2-aminoethoxy)ethoxy}ethyl] β-lactoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-[2-(2-azidoethoxy)ethoxy]ethanol (86520-52-7) → 1-[2-{2-(2-aminoethoxy)ethoxy}ethyl] β-lactoside (879004-80-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 82 percent / HgO; HgBr₂; MS 4A / CHCl₃ / 48 h / 20 °C

2: 100 percent / NaOMe / methanol / 3 h / 0 °C / pH 10

3: hydrogen / PtO₂ / methanol / 1 h / 2585.74 Torr

With hydrogen; sodium methylate; mercury dibromide; mercury(II) oxide; platinum(IV) oxide; In methanol; chloroform; 1: Koeenigs-Knorr glycosylation / 2: Zemplen deacetylation / 3: Catalytic hydrogenation;

DOI:10.1016/S0968-0896(99)00099-1

upstream raw materials:

2-[2-(2-azidoethoxy)ethoxy]ethanol