N-(2-{2-phenyl-6-[4-(3-phenylprop-2-ynyl)piperazine-1-carbonyl]-7H-pyrrolo[2,3-d]pyrimidin-4-ylamino}ethyl)acetamide

Base Information

• Chemical Name: N-(2-{2-phenyl-6-[4-(3-phenylprop-2-ynyl)piperazine-1-carbonyl]-7H-pyrrolo[2,3-d]pyrimidin-4-ylamino}ethyl)acetamide
• CAS No.: 553633-05-9
• Molecular Formula: C₃₀H₃₁N₇O₂
• Molecular Weight: 521.622

Synonyms:N-(2-{2-phenyl-6-[4-(3-phenylprop-2-ynyl)piperazine-1-carbonyl]-7H-pyrrolo[2,3-d]pyrimidin-4-ylamino}ethyl)acetamide

Chemical Property of N-(2-{2-phenyl-6-[4-(3-phenylprop-2-ynyl)piperazine-1-carbonyl]-7H-pyrrolo[2,3-d]pyrimidin-4-ylamino}ethyl)acetamide

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Technology Process of N-(2-{2-phenyl-6-[4-(3-phenylprop-2-ynyl)piperazine-1-carbonyl]-7H-pyrrolo[2,3-d]pyrimidin-4-ylamino}ethyl)acetamide

There total 2 articles about N-(2-{2-phenyl-6-[4-(3-phenylprop-2-ynyl)piperazine-1-carbonyl]-7H-pyrrolo[2,3-d]pyrimidin-4-ylamino}ethyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

4-(2-acetylaminoethylamino)-2-phenyl-7H-pyrrolo[2;3-d]pyrimidine-6-carboxylic acid (553632-82-9) + O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate (125700-67-6) + 1-(3-phenylprop-2-yn-1-yl)piperazine (148728-47-6) → N-(2-{2-phenyl-6-[4-(3-phenylprop-2-ynyl)piperazine-1-carbonyl]-7H-pyrrolo[2,3-d]pyrimidin-4-ylamino}ethyl)acetamide (553633-05-9)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃;

DOI:10.1016/j.bcp.2004.03.026

Reference yield:

→ N-(2-{2-phenyl-6-[4-(3-phenylprop-2-ynyl)piperazine-1-carbonyl]-7H-pyrrolo[2,3-d]pyrimidin-4-ylamino}ethyl)acetamide (553633-05-9)

Guidance literature:

Reference yield: 72.0%

N-(2-{2-phenyl-6-[4-(3-phenylprop-2-ynyl)piperazine-1-carbonyl]-7H-pyrrolo[2,3-d]pyrimidin-4-ylamino}ethyl)acetamide (553633-05-9) → [3H]-OSIP339391

Guidance literature:

With Pd-BaSO₄; tritium; In methanol; at 20 ℃; for 5h;

DOI:10.1016/j.bcp.2004.03.026

upstream raw materials:

4-(2-acetylaminoethylamino)-2-phenyl-7H-pyrrolo[2;3-d]pyrimidine-6-carboxylic acid

O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate

1-(3-phenylprop-2-yn-1-yl)piperazine

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