7-(3-(benzyloxy)-4-methoxyphenyl)-1-(4-bromophenyl)-5-hydroxyheptan-3-one

Base Information

Chemical Name:7-(3-(benzyloxy)-4-methoxyphenyl)-1-(4-bromophenyl)-5-hydroxyheptan-3-one
CAS No.:1426838-64-3
Molecular Formula:C₂₇H₂₉BrO₄
Molecular Weight:497.429
Hs Code.:

Synonyms:7-(3-(benzyloxy)-4-methoxyphenyl)-1-(4-bromophenyl)-5-hydroxyheptan-3-one

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Chemical Property of 7-(3-(benzyloxy)-4-methoxyphenyl)-1-(4-bromophenyl)-5-hydroxyheptan-3-one

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Technology Process of 7-(3-(benzyloxy)-4-methoxyphenyl)-1-(4-bromophenyl)-5-hydroxyheptan-3-one

There total 1 articles about 7-(3-(benzyloxy)-4-methoxyphenyl)-1-(4-bromophenyl)-5-hydroxyheptan-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 3-(3-(benzyloxy)-4-methoxyphenyl)propanal

: 89201-84-3
4-(4-bromophenyl)-2-butanone

: 1426838-64-3
7-(3-(benzyloxy)-4-methoxyphenyl)-1-(4-bromophenyl)-5-hydroxyheptan-3-one

Guidance literature:: 4-(4-bromophenyl)-2-butanone; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

3-(3-(benzyloxy)-4-methoxyphenyl)propanal; In tetrahydrofuran; hexane; at -78 ℃; for 2.5h; Inert atmosphere;
DOI:10.1021/jo400157d

Reference yield:

: 1426838-64-3
7-(3-(benzyloxy)-4-methoxyphenyl)-1-(4-bromophenyl)-5-hydroxyheptan-3-one

: 1426838-65-4
C₂₇H₂₇BrO₄

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In ethyl acetate; Reflux; Inert atmosphere;
DOI:10.1021/jo400157d

Reference yield:

: 1426838-64-3
7-(3-(benzyloxy)-4-methoxyphenyl)-1-(4-bromophenyl)-5-hydroxyheptan-3-one

: 1426838-49-4
C₂₀H₂₁BrO₄

Guidance literature:: Multi-step reaction with 2 steps

1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / Reflux; Inert atmosphere

2: pentamethylbenzene,; boron trichloride / dichloromethane / 0.17 h / -78 °C / Inert atmosphere

With pentamethylbenzene,; boron trichloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dichloromethane; ethyl acetate;
DOI:10.1021/jo400157d