16-(3-chlorophenyl)-3,3-dimethyl-2,3,4,16-tetrahydro-1H-benzo[a]chromeno[2,3-c]phenazin-1-one

Base Information

Chemical Name:16-(3-chlorophenyl)-3,3-dimethyl-2,3,4,16-tetrahydro-1H-benzo[a]chromeno[2,3-c]phenazin-1-one
CAS No.:1392831-10-5
Molecular Formula:C₃₁H₂₃ClN₂O₂
Molecular Weight:490.989
Hs Code.:

Synonyms:16-(3-chlorophenyl)-3,3-dimethyl-2,3,4,16-tetrahydro-1H-benzo[a]chromeno[2,3-c]phenazin-1-one

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Chemical Property of 16-(3-chlorophenyl)-3,3-dimethyl-2,3,4,16-tetrahydro-1H-benzo[a]chromeno[2,3-c]phenazin-1-one

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Technology Process of 16-(3-chlorophenyl)-3,3-dimethyl-2,3,4,16-tetrahydro-1H-benzo[a]chromeno[2,3-c]phenazin-1-one

There total 4 articles about 16-(3-chlorophenyl)-3,3-dimethyl-2,3,4,16-tetrahydro-1H-benzo[a]chromeno[2,3-c]phenazin-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 225-61-6
1,2-benzophenazine

: 126-81-8
dimedone

: 587-04-2
m-Chlorobenzaldehyde

: 1392831-10-5
16-(3-chlorophenyl)-3,3-dimethyl-2,3,4,16-tetrahydro-1H-benzo[a]chromeno[2,3-c]phenazin-1-one

Guidance literature:: With fulvic acid; In water; at 60 ℃; for 3h; Green chemistry;
DOI:10.1080/00304948.2019.1697608

Reference yield:

: 95-54-5
1,2-diamino-benzene

: 1392831-10-5
16-(3-chlorophenyl)-3,3-dimethyl-2,3,4,16-tetrahydro-1H-benzo[a]chromeno[2,3-c]phenazin-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / PEG-400 / 0.5 h / 70 °C

2: PEG-400 / 2 h / 70 °C

With toluene-4-sulfonic acid; In PEG-400;
DOI:10.1039/c2gc35644a

Reference yield:

: 83-72-7
2-hydroxynaphtho-1,4-quinone

: 1392831-10-5
16-(3-chlorophenyl)-3,3-dimethyl-2,3,4,16-tetrahydro-1H-benzo[a]chromeno[2,3-c]phenazin-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / PEG-400 / 0.5 h / 70 °C

2: PEG-400 / 2 h / 70 °C

With toluene-4-sulfonic acid; In PEG-400;
DOI:10.1039/c2gc35644a