C₂₅H₂₄N₂O₃

Base Information

Chemical Name:C₂₅H₂₄N₂O₃
CAS No.:313948-11-7
Molecular Formula:C₂₅H₂₄N₂O₃
Molecular Weight:400.477
Hs Code.:

C<sub>25</sub>H<sub>24</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₅H₂₄N₂O₃

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Chemical Property of C₂₅H₂₄N₂O₃

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Technology Process of C₂₅H₂₄N₂O₃

There total 7 articles about C₂₅H₂₄N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 313948-08-2
(1S,6R)-7-benzyl-9-methylene-8-oxo-7-azabicyclo[4.2.1]non-3-ene-4-carboxylic acid methoxymethyl-(2-bromophenyl)amide

: 313948-11-7
C₂₅H₂₄N₂O₃

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In acetonitrile; at 110 ℃; for 42h;
DOI:10.1021/jo001119t

Reference yield:

: 615-36-1
2-bromoaniline

: 313948-11-7
C₂₅H₂₄N₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1: 64 percent / Pd(OAc)2; triphenylphosphine; triethylamine / dimethylformamide / 20 h / 40 °C

2: 66 percent / PCC / CH₂Cl₂ / 17 h / 40 °C

3: 83 percent / n-BuLi / tetrahydrofuran; hexane / 18 h / 70 °C

4: 73 percent / sodium hydride / tetrahydrofuran; various solvent(s) / 18 h / 20 °C

5: 84 percent / Pd(PPh₃)4; triethylamine / acetonitrile / 42 h / 110 °C

With palladium diacetate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; sodium hydride; triethylamine; triphenylphosphine; pyridinium chlorochromate; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 3: Wittig reaction / 5: Heck cyclization;
DOI:10.1021/jo001119t

Reference yield:

: 199103-44-1
1-benzyl-5-ethoxy-4-hydroxy-3-(buta-2,3-dienyl)-2-pyrrolidinone

: 313948-11-7
C₂₅H₂₄N₂O₃

Guidance literature:: Multi-step reaction with 6 steps

1: 42 percent / sodium iodide / 18 h / 85 °C

2: 64 percent / Pd(OAc)2; triphenylphosphine; triethylamine / dimethylformamide / 20 h / 40 °C

3: 66 percent / PCC / CH₂Cl₂ / 17 h / 40 °C

4: 83 percent / n-BuLi / tetrahydrofuran; hexane / 18 h / 70 °C

5: 73 percent / sodium hydride / tetrahydrofuran; various solvent(s) / 18 h / 20 °C

6: 84 percent / Pd(PPh₃)4; triethylamine / acetonitrile / 42 h / 110 °C

With palladium diacetate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; sodium hydride; triethylamine; triphenylphosphine; pyridinium chlorochromate; sodium iodide; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 4: Wittig reaction / 6: Heck cyclization;
DOI:10.1021/jo001119t