(2S,3R,4S)-4-Ethyl-5-oxo-2-phenyl-tetrahydro-furan-3-carbaldehyde O-benzyl-oxime

Base Information

Chemical Name:(2S,3R,4S)-4-Ethyl-5-oxo-2-phenyl-tetrahydro-furan-3-carbaldehyde O-benzyl-oxime
CAS No.:870716-68-0
Molecular Formula:C₂₀H₂₁NO₃
Molecular Weight:323.392
Hs Code.:

Synonyms:(2S,3R,4S)-4-Ethyl-5-oxo-2-phenyl-tetrahydro-furan-3-carbaldehyde O-benzyl-oxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R,4S)-4-Ethyl-5-oxo-2-phenyl-tetrahydro-furan-3-carbaldehyde O-benzyl-oxime

Chemical Property:

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Technology Process of (2S,3R,4S)-4-Ethyl-5-oxo-2-phenyl-tetrahydro-furan-3-carbaldehyde O-benzyl-oxime

There total 1 articles about (2S,3R,4S)-4-Ethyl-5-oxo-2-phenyl-tetrahydro-furan-3-carbaldehyde O-benzyl-oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (E)-4-((1R,5S,7S)-10,10-Dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1,5]dec-4-yl)-4-oxo-but-2-enal O-benzyl-oxime

: 97-94-9
triethyl borane

: 100-52-7
benzaldehyde

: 870716-68-0
(2S,3R,4S)-4-Ethyl-5-oxo-2-phenyl-tetrahydro-furan-3-carbaldehyde O-benzyl-oxime

Guidance literature:: With trimethylaluminum; In hexane; dichloromethane; Heating;
DOI:10.1002/anie.200502263

Reference yield: 68.0%

: 870716-68-0
(2S,3R,4S)-4-Ethyl-5-oxo-2-phenyl-tetrahydro-furan-3-carbaldehyde O-benzyl-oxime

: 100-46-9
benzylamine

: 870716-73-7
(2S,3R,4S)-N-Benzyl-3-(benzyloxyimino-methyl)-2-ethyl-4-hydroxy-4-phenyl-butyramide

Guidance literature:: With 2-hydroxypyridin;
DOI:10.1002/anie.200502263

Reference yield:

: 870716-68-0
(2S,3R,4S)-4-Ethyl-5-oxo-2-phenyl-tetrahydro-furan-3-carbaldehyde O-benzyl-oxime

: (2S,3R,4S)-N-Benzyl-3-(benzyloxyamino-methyl)-2-ethyl-4-hydroxy-4-phenyl-butyramide

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / 2-pyridinol

2: 35 percent / NaBH₃CN; HCl

With 2-hydroxypyridin; hydrogenchloride; sodium cyanoborohydride;
DOI:10.1002/anie.200502263