N-[(1S,2R)-2-hydroxy-3,3-dimethyl-1-phenylbutyl]-P,P-diphenyl-N-[(1S)-1-phenylethyl]phosphinic amide

Base Information

Chemical Name:N-[(1S,2R)-2-hydroxy-3,3-dimethyl-1-phenylbutyl]-P,P-diphenyl-N-[(1S)-1-phenylethyl]phosphinic amide
CAS No.:1010128-99-0
Molecular Formula:C₃₂H₃₆NO₂P
Molecular Weight:497.617
Hs Code.:

Synonyms:N-[(1S,2R)-2-hydroxy-3,3-dimethyl-1-phenylbutyl]-P,P-diphenyl-N-[(1S)-1-phenylethyl]phosphinic amide

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Chemical Property of N-[(1S,2R)-2-hydroxy-3,3-dimethyl-1-phenylbutyl]-P,P-diphenyl-N-[(1S)-1-phenylethyl]phosphinic amide

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Technology Process of N-[(1S,2R)-2-hydroxy-3,3-dimethyl-1-phenylbutyl]-P,P-diphenyl-N-[(1S)-1-phenylethyl]phosphinic amide

There total 2 articles about N-[(1S,2R)-2-hydroxy-3,3-dimethyl-1-phenylbutyl]-P,P-diphenyl-N-[(1S)-1-phenylethyl]phosphinic amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: P,P-diphenyl-N-[(1S)-1-phenylethyl]-N-[(R)-phenyl(trimethylstannyl)methyl]phosphinic amide

: 630-19-3
pivalaldehyde

: 1010128-99-0
N-[(1S,2R)-2-hydroxy-3,3-dimethyl-1-phenylbutyl]-P,P-diphenyl-N-[(1S)-1-phenylethyl]phosphinic amide

Guidance literature:: P,P-diphenyl-N-[(1S)-1-phenylethyl]-N-[(R)-phenyl(trimethylstannyl)methyl]phosphinic amide; With sec.-butyllithium; In diethyl ether; at -90 ℃; for 0.166667h;

pivalaldehyde; In diethyl ether; at -90 ℃; for 0.0833333h; Further stages.;
DOI:10.1021/ol7028096

Reference yield: 95.0%

: 1010128-68-3
N-benzyl-P,P-diphenyl-N-[(1S)-1-phenylethyl]phosphinic amide

: 630-19-3
pivalaldehyde

: 1010128-99-0
N-[(1S,2R)-2-hydroxy-3,3-dimethyl-1-phenylbutyl]-P,P-diphenyl-N-[(1S)-1-phenylethyl]phosphinic amide

Guidance literature:: N-benzyl-P,P-diphenyl-N-[(1S)-1-phenylethyl]phosphinic amide; With tert.-butyl lithium; In diethyl ether; hexane; at -90 ℃; for 2h;

pivalaldehyde; In diethyl ether; hexane; at -90 ℃; for 0.5h; Further stages.;
DOI:10.1021/ol7028096