4-phenyl-3-buten-1-yl 3,3-dimethyl-2-phenylcyclopropenecarboxylate

Base Information

Chemical Name:4-phenyl-3-buten-1-yl 3,3-dimethyl-2-phenylcyclopropenecarboxylate
CAS No.:99376-56-4
Molecular Formula:C₂₂H₂₂O₂
Molecular Weight:318.415
Hs Code.:

Synonyms:4-phenyl-3-buten-1-yl 3,3-dimethyl-2-phenylcyclopropenecarboxylate

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Chemical Property of 4-phenyl-3-buten-1-yl 3,3-dimethyl-2-phenylcyclopropenecarboxylate

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Technology Process of 4-phenyl-3-buten-1-yl 3,3-dimethyl-2-phenylcyclopropenecarboxylate

There total 3 articles about 4-phenyl-3-buten-1-yl 3,3-dimethyl-2-phenylcyclopropenecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 770-36-5,20047-19-2,937-58-6
4-phenylbuta-3-en-1-ol

: 99376-68-8
3,3-dimethyl-2-phenyl-cyclopropenecarboxylic acid

: 99376-56-4
4-phenyl-3-buten-1-yl 3,3-dimethyl-2-phenylcyclopropenecarboxylate

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In diethyl ether; for 12h;
DOI:10.1021/jo00225a064

Reference yield:

: 2243-53-0
styrylacetic acid

: 99376-56-4
4-phenyl-3-buten-1-yl 3,3-dimethyl-2-phenylcyclopropenecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / LiAlH₄ / diethyl ether / 18 h / Heating

2: 64 percent / triphenylphosphine, diethyl azodicarboxylate / diethyl ether / 12 h

With lithium aluminium tetrahydride; triphenylphosphine; diethylazodicarboxylate; In diethyl ether;
DOI:10.1021/jo00225a064

Reference yield:

: 21603-24-7
methyl 3,3-dimethyl-1-phenylcyclopropene-2-carboxylate

: 99376-56-4
4-phenyl-3-buten-1-yl 3,3-dimethyl-2-phenylcyclopropenecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / KOH, H₂O / propan-2-ol / 36 h / Heating

2: 64 percent / triphenylphosphine, diethyl azodicarboxylate / diethyl ether / 12 h

With potassium hydroxide; water; triphenylphosphine; diethylazodicarboxylate; In diethyl ether; isopropyl alcohol;
DOI:10.1021/jo00225a064