[3-(dimethylcarbamoyl)-4-{[(4'-isopropoxybiphenyl-2-yl)carbonyl]amino}phenyl]acetic acid

Base Information

Chemical Name:[3-(dimethylcarbamoyl)-4-{[(4'-isopropoxybiphenyl-2-yl)carbonyl]amino}phenyl]acetic acid
CAS No.:1350469-53-2
Molecular Formula:C₂₇H₂₈N₂O₅
Molecular Weight:460.53
Hs Code.:

Synonyms:[3-(dimethylcarbamoyl)-4-{[(4'-isopropoxybiphenyl-2-yl)carbonyl]amino}phenyl]acetic acid

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Chemical Property of [3-(dimethylcarbamoyl)-4-{[(4'-isopropoxybiphenyl-2-yl)carbonyl]amino}phenyl]acetic acid

Chemical Property:

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Technology Process of [3-(dimethylcarbamoyl)-4-{[(4'-isopropoxybiphenyl-2-yl)carbonyl]amino}phenyl]acetic acid

There total 5 articles about [3-(dimethylcarbamoyl)-4-{[(4'-isopropoxybiphenyl-2-yl)carbonyl]amino}phenyl]acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1350469-52-1
diethyl [3-(dimethylcarbamoyl)-4-{[(4'-isopropoxybiphenyl-2-yl)carbonyl]amino}phenyl]malonate

: 1350469-53-2
[3-(dimethylcarbamoyl)-4-{[(4'-isopropoxybiphenyl-2-yl)carbonyl]amino}phenyl]acetic acid

Guidance literature:: diethyl [3-(dimethylcarbamoyl)-4-{[(4'-isopropoxybiphenyl-2-yl)carbonyl]amino}phenyl]malonate; With water; potassium carbonate; In tetrahydrofuran; methanol; for 7h; Reflux;

With hydrogenchloride; In methanol; water; pH=2;

Reference yield:

: 408366-55-2
4’-isopropoxy-2-biphenylcarboxylic acid

: 1350469-53-2
[3-(dimethylcarbamoyl)-4-{[(4'-isopropoxybiphenyl-2-yl)carbonyl]amino}phenyl]acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / 2-methyltetrahydrofuran / 1.5 h / 20 °C

3.1: potassium carbonate; water / tetrahydrofuran; methanol / 7 h / Reflux

3.2: pH 2

With oxalyl dichloride; water; potassium carbonate; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; In tetrahydrofuran; 2-methyltetrahydrofuran; methanol; dichloromethane;

Reference yield:

: C₁₆H₁₅ClO₂

: 1350469-53-2
[3-(dimethylcarbamoyl)-4-{[(4'-isopropoxybiphenyl-2-yl)carbonyl]amino}phenyl]acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine / 2-methyltetrahydrofuran / 1.5 h / 20 °C

2.1: potassium carbonate; water / tetrahydrofuran; methanol / 7 h / Reflux

2.2: pH 2

With water; potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 2-methyltetrahydrofuran; methanol;