1-benzyl-2-chloro-3-phenylsulfinylindole

Base Information

Chemical Name:1-benzyl-2-chloro-3-phenylsulfinylindole
CAS No.:108698-77-7
Molecular Formula:C₂₁H₁₆ClNOS
Molecular Weight:365.883
Hs Code.:

Synonyms:1-benzyl-2-chloro-3-phenylsulfinylindole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-benzyl-2-chloro-3-phenylsulfinylindole

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Technology Process of 1-benzyl-2-chloro-3-phenylsulfinylindole

There total 5 articles about 1-benzyl-2-chloro-3-phenylsulfinylindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 98508-72-6
1-Benzyl-2-chloro-3-phenylthioindole

: 108698-77-7
1-benzyl-2-chloro-3-phenylsulfinylindole

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; for 0.333333h;
DOI:10.1021/jo00246a048

Reference yield:

: 54491-43-9
3-phenylthioindole

: 108698-77-7
1-benzyl-2-chloro-3-phenylsulfinylindole

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / m-chloroperoxybenzoic acid / CH₂Cl₂ / 0.08 h / 0 °C

2: 1.) NaH / 1.) DMF, 0 deg C, 30 min, 2.) 5 min

3: 94 percent / NaHCO₃, SOCl₂ / CH₂Cl₂ / 0 °C

4: 84 percent / m-chloroperoxybenzoic acid / CH₂Cl₂ / 0.33 h / 0 - 20 °C

With thionyl chloride; sodium hydride; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jo00246a048

Reference yield:

: 98508-67-9
3-(phenylsulfinyl)-1H-indole

: 108698-77-7
1-benzyl-2-chloro-3-phenylsulfinylindole

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) DMF, 0 deg C, 30 min, 2.) 5 min

2: 94 percent / NaHCO₃, SOCl₂ / CH₂Cl₂ / 0 °C

3: 84 percent / m-chloroperoxybenzoic acid / CH₂Cl₂ / 0.33 h / 0 - 20 °C

With thionyl chloride; sodium hydride; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jo00246a048