Technology Process of C28H29NO5Si
There total 7 articles about C28H29NO5Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium on activated charcoal; hydrogen;
In
methanol;
at 20 ℃;
DOI:10.1021/op3001383
- Guidance literature:
-
Multi-step reaction with 6 steps
1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane
2: n-butyllithium / tetrahydrofuran / 0 - 20 °C
3: triethylamine; titanium tetrachloride / dichloromethane / -10 - 0 °C
4: 1H-imidazole / dichloromethane / 20 °C
5: n-butyllithium / tetrahydrofuran / -35 - -30 °C
6: hydrogen; palladium on activated charcoal / methanol / 20 °C
With
1H-imidazole; n-butyllithium; oxalyl dichloride; palladium on activated charcoal; hydrogen; titanium tetrachloride; triethylamine; N,N-dimethyl-formamide;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/op3001383
- Guidance literature:
-
Multi-step reaction with 5 steps
1: n-butyllithium / tetrahydrofuran / 0 - 20 °C
2: triethylamine; titanium tetrachloride / dichloromethane / -10 - 0 °C
3: 1H-imidazole / dichloromethane / 20 °C
4: n-butyllithium / tetrahydrofuran / -35 - -30 °C
5: hydrogen; palladium on activated charcoal / methanol / 20 °C
With
1H-imidazole; n-butyllithium; palladium on activated charcoal; hydrogen; titanium tetrachloride; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/op3001383
