Technology Process of Zn(II)(Ph3C20H8N4C6H4CONHC6H4C6H4NH2)
There total 5 articles about Zn(II)(Ph3C20H8N4C6H4CONHC6H4C6H4NH2) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
zinc diacetate;
In
methanol; chloroform;
for 2h;
Reflux;
Inert atmosphere;
DOI:10.1039/c2ob25147g
- Guidance literature:
-
In
methanol; chloroform;
addn. of porphyrin deriv. to soln. of zinc acetate in CHCl3/methanol (2:1), refluxing for 2 h in dark; cooling to room temp., washing with water, drying over Na2SO4, evapn., NMR and MS;
DOI:10.1039/c2ob25147g
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 48 h / 20 °C
2: tetrakis(triphenylphosphine) palladium(0); potassium hydroxide / tetrahydrofuran; water / 1.5 h / Inert atmosphere; Reflux; Darkness
3: zinc diacetate / methanol; chloroform / 2 h / Reflux; Inert atmosphere
With
pyridine; tetrakis(triphenylphosphine) palladium(0); zinc diacetate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide;
In
tetrahydrofuran; methanol; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1039/c2ob25147g
