Technology Process of C24H39N5O8S2
There total 11 articles about C24H39N5O8S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tert-butyl alcohol;
In
dichloromethane;
for 4h;
DOI:10.1021/jm9900321
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 72 percent / Et3N / tetrahydrofuran; H2O / 3.5 h / 20 °C
2: 83 percent / aq. NaOH; Br2 / 1 h / 85 °C
3: 63 percent / H2SO4 / dioxane / 114 h
4: 94 percent / N-methylmorpholine; BOP / dioxane / 18 h / 20 °C
5: 83 percent / Ph3P; aq. NH3 / dioxane
6: 20 percent / t-BuOH / CH2Cl2 / 4 h
With
4-methyl-morpholine; ammonium hydroxide; sodium hydroxide; sulfuric acid; bromine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; triphenylphosphine; tert-butyl alcohol;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
1: sulfonylation / 2: Hoffmann's degradation / 3: Esterification / 4: Condensation / 5: Reduction / 6: Condensation;
DOI:10.1021/jm9900321
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 86 percent / aq. NaHCO3 / tetrahydrofuran / 0 - 20 °C
2: 90 percent / pyridine / CH2Cl2 / 18 h / 20 °C
3: 92 percent / NaN3 / dimethylformamide
4: 86 percent / aq. NaOH / ethanol / 2 h / 20 °C
5: 94 percent / N-methylmorpholine; BOP / dioxane / 18 h / 20 °C
6: 83 percent / Ph3P; aq. NH3 / dioxane
7: 20 percent / t-BuOH / CH2Cl2 / 4 h
With
4-methyl-morpholine; pyridine; ammonium hydroxide; sodium hydroxide; sodium azide; sodium hydrogencarbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triphenylphosphine; tert-butyl alcohol;
In
tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; N,N-dimethyl-formamide;
1: cyclocondensation / 2: Tosylation / 3: Substitution / 4: Hydrolysis / 5: Condensation / 6: Reduction / 7: Condensation;
DOI:10.1021/jm9900321