C₁₄H₁₈O₅

Base Information

Chemical Name:C₁₄H₁₈O₅
CAS No.:1347703-98-3
Molecular Formula:C₁₄H₁₈O₅
Molecular Weight:266.294
Hs Code.:

C<sub>14</sub>H<sub>18</sub>O<sub>5</sub>

Synonyms:C₁₄H₁₈O₅

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Chemical Property of C₁₄H₁₈O₅

Chemical Property:

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Technology Process of C₁₄H₁₈O₅

There total 10 articles about C₁₄H₁₈O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1347703-97-2
C₃₀H₃₄O₆

: 1347703-98-3
C₁₄H₁₈O₅

Guidance literature:: With titanium tetrachloride; In dichloromethane; at 0 - 20 ℃; for 15h;
DOI:10.1016/j.tetlet.2011.09.105

Reference yield:

: 100-52-7
benzaldehyde

: 1347703-98-3
C₁₄H₁₈O₅

Guidance literature:: Multi-step reaction with 10 steps

1.1: titanium(IV) isopropylate; (S)-[1,1']-binaphthalenyl-2,2'-diol / dichloromethane / 0.17 h / 20 °C

1.2: 24 h / -78 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 15 h / 0 - 20 °C

3.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 24 h / 20 °C

4.1: sodium periodate / tetrahydrofuran; water

5.1: L-proline / chloroform / 4 h / 0 °C

5.2: 1.5 h / 20 °C

6.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 12 h / 0 - 20 °C

7.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 24 h / 20 °C

8.1: sodium periodate / tetrahydrofuran; water

9.1: sodium hydride / tetrahydrofuran / 1 h / -78 °C

10.1: titanium tetrachloride / dichloromethane / 15 h / 0 - 20 °C

With titanium(IV) isopropylate; sodium periodate; osmium(VIII) oxide; (S)-[1,1']-binaphthalenyl-2,2'-diol; titanium tetrachloride; tetra-(n-butyl)ammonium iodide; sodium hydride; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; L-proline; In tetrahydrofuran; dichloromethane; chloroform; water; acetone; 1.2: Keck allylation / 9.1: Horner-Wadsworth-Emmons olefination;
DOI:10.1016/j.tetlet.2011.09.105

Reference yield:

: 1347703-89-2
C₁₂H₁₆O₂

: 1347703-98-3
C₁₄H₁₈O₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 24 h / 20 °C

2.1: sodium periodate / tetrahydrofuran; water

3.1: L-proline / chloroform / 4 h / 0 °C

3.2: 1.5 h / 20 °C

4.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 12 h / 0 - 20 °C

5.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 24 h / 20 °C

6.1: sodium periodate / tetrahydrofuran; water

7.1: sodium hydride / tetrahydrofuran / 1 h / -78 °C

8.1: titanium tetrachloride / dichloromethane / 15 h / 0 - 20 °C

With sodium periodate; osmium(VIII) oxide; titanium tetrachloride; tetra-(n-butyl)ammonium iodide; sodium hydride; 4-methylmorpholine N-oxide; L-proline; In tetrahydrofuran; dichloromethane; chloroform; water; acetone; 7.1: Horner-Wadsworth-Emmons olefination;
DOI:10.1016/j.tetlet.2011.09.105