Technology Process of C32H38O10
There total 4 articles about C32H38O10 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 93 percent / tetrapropylammonium perruthenate, 4-methylmorpholine N-oxide / acetonitrile / 2 h / 25 °C
2: p-toluenesulfonic acid / methanol / 48 h / 25 °C
3: 1.) Dess-Martin periodinane, 2.) 4-(dimethylamino)pyridine, 3.) n-Bu4NBH4
With
dmap; tetrapropylammonium perruthennate; tetrabutylammonium borohydride; Dess-Martin periodane; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide;
In
methanol; acetonitrile;
DOI:10.1021/ja00107a009
- Guidance literature:
-
Multi-step reaction with 2 steps
1: p-toluenesulfonic acid / methanol / 48 h / 25 °C
2: 1.) Dess-Martin periodinane, 2.) 4-(dimethylamino)pyridine, 3.) n-Bu4NBH4
With
dmap; tetrabutylammonium borohydride; Dess-Martin periodane; toluene-4-sulfonic acid;
In
methanol;
DOI:10.1021/ja00107a009
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 95 percent / 4-(dimethylamino)pyridine / CH2Cl2 / 2 h / 25 °C
2: 93 percent / tetrapropylammonium perruthenate, 4-methylmorpholine N-oxide / acetonitrile / 2 h / 25 °C
3: p-toluenesulfonic acid / methanol / 48 h / 25 °C
4: 1.) Dess-Martin periodinane, 2.) 4-(dimethylamino)pyridine, 3.) n-Bu4NBH4
With
dmap; tetrapropylammonium perruthennate; tetrabutylammonium borohydride; Dess-Martin periodane; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide;
In
methanol; dichloromethane; acetonitrile;
DOI:10.1021/ja00107a009
