CID 11342154

Base Information

Chemical Name:CID 11342154
CAS No.:79982-56-2
Molecular Formula:C20H16 Cl2 N4 Os
Molecular Weight:591.495
Hs Code.:
Mol file:79982-56-2.mol

Synonyms:SCHEMBL4484459

Suppliers and Price of CID 11342154

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 11 raw suppliers

Chemical Property of CID 11342154

Chemical Property:

Boiling Point:272.5oC at 760 mmHg
Flash Point:107.2oC
PSA：51.56000
LogP:-7.69680
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:574.03668
Heavy Atom Count:27
Complexity:123

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=NC(=C1)C2=CC=CC=N2.C1=CC=NC(=C1)C2=CC=CC=N2.Cl[Os]Cl

Technology Process of CID 11342154

There total 17 articles about CID 11342154 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 13444-93-4
osmium(III) chloride

: 79982-56-2
cis-[bis(2,2'-bipyridine)dichloridoosmium(II)]

Guidance literature:: With LiCl, Bipy; In N,N-dimethyl-formamide; to the soln. of LiCl with gentle warming OsCl3 and Bipy were added under N2, the mixt. was refluxed for 2 h; the soln. was cooled to 25°C, acetone was added, the mixt. was cooled to 0°C, ppt. was filtered off, washed with water, dried in vac. at 25°C for 12 h, elem. anal.;

Reference yield: 87.0%

: 366-18-7
[2,2]bipyridinyl

: potassium hexachloroosmate(IV)

: 15702-72-4,79982-56-2
bis(2,2'-bipyridine)osmium(II) dichloride

Guidance literature:: [2,2]bipyridinyl; potassium hexachloroosmate(IV); In DMF (N,N-dimethyl-formamide); for 1h; Heating / reflux;

With sodium dithionite; In DMF (N,N-dimethyl-formamide); water; at 20 ℃;

Reference yield: 87.0%

: 366-18-7
[2,2]bipyridinyl

: 1307-81-9
Na₂OsCl₆*xH₂O

: 23648-06-8,24191-05-7,174291-50-0
tris(2,2'-bipyridine)osmium(II)

: 79982-56-2
cis-[bis(2,2'-bipyridine)dichloridoosmium(II)]

Guidance literature:: With sodium dithionite; In water; ethylene glycol; (N2); refluxing the Os salt and 2,2'-bipyridyl in ethylene glycol for 45min, cooling, addn. of satd. aq. sodium dithionite; filtration, washing (H2O; Et2O); elem. anal.;