(2E,2'E)-N,N'-(2,2'-disulfanediylbis(ethane-2,1-diyl))bis(3-(4-(benzyloxy)-3-bromophenyl)-2-(benzyloxyimino)propanamide)

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Chemical Name:(2E,2'E)-N,N'-(2,2'-disulfanediylbis(ethane-2,1-diyl))bis(3-(4-(benzyloxy)-3-bromophenyl)-2-(benzyloxyimino)propanamide)
CAS No.:1415814-16-2
Molecular Formula:C₅₀H₄₈Br₂N₄O₆S₂
Molecular Weight:1024.89
Hs Code.:

Synonyms:(2E,2'E)-N,N'-(2,2'-disulfanediylbis(ethane-2,1-diyl))bis(3-(4-(benzyloxy)-3-bromophenyl)-2-(benzyloxyimino)propanamide)

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Chemical Property of (2E,2'E)-N,N'-(2,2'-disulfanediylbis(ethane-2,1-diyl))bis(3-(4-(benzyloxy)-3-bromophenyl)-2-(benzyloxyimino)propanamide)

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Technology Process of (2E,2'E)-N,N'-(2,2'-disulfanediylbis(ethane-2,1-diyl))bis(3-(4-(benzyloxy)-3-bromophenyl)-2-(benzyloxyimino)propanamide)

There total 4 articles about (2E,2'E)-N,N'-(2,2'-disulfanediylbis(ethane-2,1-diyl))bis(3-(4-(benzyloxy)-3-bromophenyl)-2-(benzyloxyimino)propanamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 3-(4-benzyloxy-3-bromo-phenyl)-2-[(Z)-benzyloxyimino]-propionic acid

: 1072-22-6
cystamine hydrochloride

: 1415814-16-2
(2E,2'E)-N,N'-(2,2'-disulfanediylbis(ethane-2,1-diyl))bis(3-(4-(benzyloxy)-3-bromophenyl)-2-(benzyloxyimino)propanamide)

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol303057a

Reference yield:

: 69455-12-5
4-benzyloxy-3-bromobenzaldehyde

: 1415814-16-2
(2E,2'E)-N,N'-(2,2'-disulfanediylbis(ethane-2,1-diyl))bis(3-(4-(benzyloxy)-3-bromophenyl)-2-(benzyloxyimino)propanamide)

Guidance literature:: Multi-step reaction with 4 steps

1: ammonium acetate / toluene / 90 - 100 °C / Inert atmosphere

2: sodium hydroxide / water / 80 - 90 °C / Inert atmosphere

3: sodium ethanolate / ethanol / 70 °C / Inert atmosphere

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / dichloromethane / 20 °C / Inert atmosphere

With ammonium acetate; sodium ethanolate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; In ethanol; dichloromethane; water; toluene;
DOI:10.1021/ol303057a

Reference yield:

: C₁₆H₁₃BrO₃S

: 1415814-16-2
(2E,2'E)-N,N'-(2,2'-disulfanediylbis(ethane-2,1-diyl))bis(3-(4-(benzyloxy)-3-bromophenyl)-2-(benzyloxyimino)propanamide)

Guidance literature:: Multi-step reaction with 2 steps

1: sodium ethanolate / ethanol / 70 °C / Inert atmosphere

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / dichloromethane / 20 °C / Inert atmosphere

With sodium ethanolate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In ethanol; dichloromethane;
DOI:10.1021/ol303057a