(Z)-5-(4-(benzyloxy)-3,5-dibromobenzylidene)-2-thioxothiazolidin-4-one

Base Information

Chemical Name:(Z)-5-(4-(benzyloxy)-3,5-dibromobenzylidene)-2-thioxothiazolidin-4-one
CAS No.:1322241-36-0
Molecular Formula:C₁₇H₁₂BrNO₂S₂
Molecular Weight:406.324
Hs Code.:

Synonyms:(Z)-5-(4-(benzyloxy)-3,5-dibromobenzylidene)-2-thioxothiazolidin-4-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-5-(4-(benzyloxy)-3,5-dibromobenzylidene)-2-thioxothiazolidin-4-one

Chemical Property:

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Technology Process of (Z)-5-(4-(benzyloxy)-3,5-dibromobenzylidene)-2-thioxothiazolidin-4-one

There total 1 articles about (Z)-5-(4-(benzyloxy)-3,5-dibromobenzylidene)-2-thioxothiazolidin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 141-84-4
2-thioxo-4-thiazolidinone

: 69455-12-5
4-benzyloxy-3-bromobenzaldehyde

: 1322241-36-0
(Z)-5-(4-(benzyloxy)-3,5-dibromobenzylidene)-2-thioxothiazolidin-4-one

Guidance literature:: With ammonium acetate; In toluene; at 90 - 100 ℃; Inert atmosphere;
DOI:10.1021/ol303057a

Reference yield:

: 1322241-36-0
(Z)-5-(4-(benzyloxy)-3,5-dibromobenzylidene)-2-thioxothiazolidin-4-one

: C₁₆H₁₃BrO₃S

Guidance literature:: With sodium hydroxide; In water; at 80 - 90 ℃; Inert atmosphere;
DOI:10.1021/ol303057a

Reference yield:

: 1322241-36-0
(Z)-5-(4-(benzyloxy)-3,5-dibromobenzylidene)-2-thioxothiazolidin-4-one

: 1415814-15-1
(E)-3-(4-(benzyloxy)-3-bromophenyl)-2-(benzyloxyimino)-N-(2-sulfamoylethyl)propanamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / water / 80 - 90 °C / Inert atmosphere

2: sodium ethanolate / ethanol / 70 °C / Inert atmosphere

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / 1,4-dioxane; methanol / 20 °C / Inert atmosphere

With sodium ethanolate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; In 1,4-dioxane; methanol; ethanol; water;
DOI:10.1021/ol303057a