C₃₃H₆₀O₃S₂Si₂

Base Information

• Chemical Name: C₃₃H₆₀O₃S₂Si₂
• CAS No.: 1380242-10-3
• Molecular Formula: C₃₃H₆₀O₃S₂Si₂
• Molecular Weight: 625.141
• Mol file: 1380242-10-3.mol

Synonyms:C₃₃H₆₀O₃S₂Si₂

Chemical Property of C₃₃H₆₀O₃S₂Si₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₃H₆₀O₃S₂Si₂

There total 5 articles about C₃₃H₆₀O₃S₂Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

C26H54O3S2Si2 (1380242-09-0) + benzyl bromide (100-39-0) → C33H60O3S2Si2 (1380242-10-3)

Guidance literature:

With sodium hexamethyldisilazane; In tetrahydrofuran; N,N-dimethyl-formamide; at -10 ℃; for 2h; Inert atmosphere;

DOI:10.1002/anie.201201395

Reference yield:

C15H30OS2Si (1306602-89-0) → C33H60O3S2Si2 (1380242-10-3)

Guidance literature:

Multi-step reaction with 2 steps

1: N,N,N,N,N,N-hexamethylphosphoric triamide; tert.-butyl lithium / tetrahydrofuran; pentane / 0.5 h / -78 - -40 °C / Inert atmosphere

2: sodium hexamethyldisilazane / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / -10 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; tert.-butyl lithium; sodium hexamethyldisilazane; In tetrahydrofuran; N,N-dimethyl-formamide; pentane;

DOI:10.1002/anie.201201395

Reference yield:

t-butyldimethylsiyl triflate (69739-34-0) → C33H60O3S2Si2 (1380242-10-3)

Guidance literature:

Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 1 h / Cooling with ice

2: N,N,N,N,N,N-hexamethylphosphoric triamide; tert.-butyl lithium / tetrahydrofuran; pentane / 0.5 h / -78 - -40 °C / Inert atmosphere

3: sodium hexamethyldisilazane / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / -10 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; tert.-butyl lithium; sodium hexamethyldisilazane; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; pentane;

DOI:10.1002/anie.201201395

upstream raw materials:

C₁₅H₃₀OS₂Si

C₁₆H₁₉NO₃S

C₉H₁₆OS₂

C₂₆H₅₄O₃S₂Si₂

Downstream raw materials:

C₃₀H₃₇NO₇

C₅₀H₆₇NO₁₁

C₅₀H₆₇NO₁₁

C₂₇H₄₆O₃S₂Si