phenyl 2-(benzyloxy)-3-[bis(prop-2-en-1-yl)amino]-5-fluoro-6-methylbenzoate

Base Information

Chemical Name:phenyl 2-(benzyloxy)-3-[bis(prop-2-en-1-yl)amino]-5-fluoro-6-methylbenzoate
CAS No.:1207284-90-9
Molecular Formula:C₂₇H₂₆FNO₃
Molecular Weight:431.507
Hs Code.:

Synonyms:phenyl 2-(benzyloxy)-3-[bis(prop-2-en-1-yl)amino]-5-fluoro-6-methylbenzoate

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Chemical Property of phenyl 2-(benzyloxy)-3-[bis(prop-2-en-1-yl)amino]-5-fluoro-6-methylbenzoate

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Technology Process of phenyl 2-(benzyloxy)-3-[bis(prop-2-en-1-yl)amino]-5-fluoro-6-methylbenzoate

There total 5 articles about phenyl 2-(benzyloxy)-3-[bis(prop-2-en-1-yl)amino]-5-fluoro-6-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1207284-89-6
phenyl 3-amino-2-(benzyloxy)-5-fluoro-6-methylbenzoate

: 106-95-6
allyl bromide

: 1207284-90-9
phenyl 2-(benzyloxy)-3-[bis(prop-2-en-1-yl)amino]-5-fluoro-6-methylbenzoate

Guidance literature:: With potassium carbonate; potassium iodide; In N-Methyl-2-pyrrolidone, NMP; at 100 ℃; for 16h; Inert atmosphere;

Reference yield:

: 1207284-87-4
phenyl 3-fluoro-6-hydroxy-2-methyl-5-nitrobenzoate

: 1207284-90-9
phenyl 2-(benzyloxy)-3-[bis(prop-2-en-1-yl)amino]-5-fluoro-6-methylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; potassium iodide / acetone / 4 h / 56 °C

2: sodium hydrosulfite / tetrahydrofuran; water / 10 - 20.4 °C

3: potassium carbonate; potassium iodide / 1-methyl-pyrrolidin-2-one / 16 h / 100 °C

With sodium hydrosulfite; potassium carbonate; potassium iodide; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; water; acetone;
DOI:10.1021/jm201467r

Reference yield:

: 1207284-88-5
phenyl 2-(benzyloxy)-5-fluoro-6-methyl-3-nitrobenzoate

: 1207284-90-9
phenyl 2-(benzyloxy)-3-[bis(prop-2-en-1-yl)amino]-5-fluoro-6-methylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrosulfite / tetrahydrofuran; water / 10 - 20.4 °C

2: potassium carbonate; potassium iodide / 1-methyl-pyrrolidin-2-one / 16 h / 100 °C

With sodium hydrosulfite; potassium carbonate; potassium iodide; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; water;
DOI:10.1021/jm201467r