7-iodo-5-chloro-6-(2,4,6-trifluorophenyl)-1,2,4-triazolo[1,5-a]pyrimidine

Base Information

Chemical Name:7-iodo-5-chloro-6-(2,4,6-trifluorophenyl)-1,2,4-triazolo[1,5-a]pyrimidine
CAS No.:1041697-24-8
Molecular Formula:C₁₁H₃ClF₃IN₄
Molecular Weight:410.524
Hs Code.:

Synonyms:7-iodo-5-chloro-6-(2,4,6-trifluorophenyl)-1,2,4-triazolo[1,5-a]pyrimidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-iodo-5-chloro-6-(2,4,6-trifluorophenyl)-1,2,4-triazolo[1,5-a]pyrimidine

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Technology Process of 7-iodo-5-chloro-6-(2,4,6-trifluorophenyl)-1,2,4-triazolo[1,5-a]pyrimidine

There total 1 articles about 7-iodo-5-chloro-6-(2,4,6-trifluorophenyl)-1,2,4-triazolo[1,5-a]pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 214707-02-5
5,7-dichloro-6-(2,4,6-trifluorophenyl)-[1,2,4]triazolo[1,5-a]pyrimidine

: 1041697-24-8
7-iodo-5-chloro-6-(2,4,6-trifluorophenyl)-1,2,4-triazolo[1,5-a]pyrimidine

Guidance literature:: With hydrogen iodide; In acetone; at 20 ℃; for 2h;
DOI:10.1016/j.tet.2008.04.084

Reference yield: 35.0%

: 1041697-24-8
7-iodo-5-chloro-6-(2,4,6-trifluorophenyl)-1,2,4-triazolo[1,5-a]pyrimidine

: 25761-72-2
N,N-diallylcarbamoyl chloride

: 1041697-42-0
5-chloro-6-(2,4,6-trifluorophenyl)-[1,2,4]triazolo[1,5-a]pyrimidine-7-carboxylic acid diallylamide

Guidance literature:: 7-iodo-5-chloro-6-(2,4,6-trifluorophenyl)-1,2,4-triazolo[1,5-a]pyrimidine; With isopropylmagnesium chloride; In tetrahydrofuran; at -23 - -20 ℃;

N,N-diallylcarbamoyl chloride; In tetrahydrofuran; at -20 - 25 ℃; Further stages.;
DOI:10.1016/j.tet.2008.04.084

Reference yield: 33.0%

: 1041697-24-8
7-iodo-5-chloro-6-(2,4,6-trifluorophenyl)-1,2,4-triazolo[1,5-a]pyrimidine

: 79-44-7
N,N-Dimethylcarbamoyl chloride

: 1041697-29-3
5-chloro-6-(2,4,6-trifluorophenyl)-[1,2,4]triazolo[1,5-a]pyrimidine-7-carboxylic acid dimethylamide

Guidance literature:: 7-iodo-5-chloro-6-(2,4,6-trifluorophenyl)-1,2,4-triazolo[1,5-a]pyrimidine; With isopropylmagnesium chloride; In tetrahydrofuran; at -23 - -20 ℃;

N,N-Dimethylcarbamoyl chloride; In tetrahydrofuran; at -20 - 25 ℃; Further stages.;
DOI:10.1016/j.tet.2008.04.084