1,11-bis<4-(2-nitrobenzamido)-2-nitrophenyl>-1,11-dioxo-6-methyl-2,6,10-triazaundecane

Base Information

Chemical Name:1,11-bis<4-(2-nitrobenzamido)-2-nitrophenyl>-1,11-dioxo-6-methyl-2,6,10-triazaundecane
CAS No.:171116-86-2
Molecular Formula:C₃₅H₃₃N₉O₁₂
Molecular Weight:771.7
Hs Code.:

Synonyms:1,11-bis<4-(2-nitrobenzamido)-2-nitrophenyl>-1,11-dioxo-6-methyl-2,6,10-triazaundecane

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Chemical Property of 1,11-bis<4-(2-nitrobenzamido)-2-nitrophenyl>-1,11-dioxo-6-methyl-2,6,10-triazaundecane

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Technology Process of 1,11-bis<4-(2-nitrobenzamido)-2-nitrophenyl>-1,11-dioxo-6-methyl-2,6,10-triazaundecane

There total 4 articles about 1,11-bis<4-(2-nitrobenzamido)-2-nitrophenyl>-1,11-dioxo-6-methyl-2,6,10-triazaundecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 105-83-9
3,3'-Diamino-N-methyldipropylamine

: 171116-85-1
4-nitrophenol 4-(2-nitrobenzamido)2-nitrobenzoate

: 171116-86-2
1,11-bis<4-(2-nitrobenzamido)-2-nitrophenyl>-1,11-dioxo-6-methyl-2,6,10-triazaundecane

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1002/poc.610080905

Reference yield:

: 610-36-6
4-amino-2-nitrobenzoic acid

: 171116-86-2
1,11-bis<4-(2-nitrobenzamido)-2-nitrophenyl>-1,11-dioxo-6-methyl-2,6,10-triazaundecane

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / Na₂CO₃ / H₂O / 0.5 h / 20 °C

2: 1.) pyridine, PCl₃ / 1.) 5 deg C, 20 deg C, 2.) reflux, 10 min

3: 79 percent / NEt₃ / dimethylformamide / 1 h / 20 °C

With pyridine; sodium carbonate; triethylamine; phosphorus trichloride; In water; N,N-dimethyl-formamide;
DOI:10.1002/poc.610080905

Reference yield:

: 171116-88-4
4-(2-nitrobenzamido)2-nitrobenzoic acid

: 171116-86-2
1,11-bis<4-(2-nitrobenzamido)-2-nitrophenyl>-1,11-dioxo-6-methyl-2,6,10-triazaundecane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) pyridine, PCl₃ / 1.) 5 deg C, 20 deg C, 2.) reflux, 10 min

2: 79 percent / NEt₃ / dimethylformamide / 1 h / 20 °C

With pyridine; triethylamine; phosphorus trichloride; In N,N-dimethyl-formamide;
DOI:10.1002/poc.610080905