Pd-Cl 3-((3,5-bis(phenylsulfanylmethyl)phenoxy)propyltrimethoxysilane

Base Information

• Chemical Name: Pd-Cl 3-((3,5-bis(phenylsulfanylmethyl)phenoxy)propyltrimethoxysilane
• CAS No.: 748150-01-8
• Molecular Formula: C₂₆H₃₁ClO₄PdS₂Si
• Molecular Weight: 641.62
• Mol file: 748150-01-8.mol

Synonyms:Pd-Cl 3-((3,5-bis(phenylsulfanylmethyl)phenoxy)propyltrimethoxysilane

Chemical Property of Pd-Cl 3-((3,5-bis(phenylsulfanylmethyl)phenoxy)propyltrimethoxysilane

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of Pd-Cl 3-((3,5-bis(phenylsulfanylmethyl)phenoxy)propyltrimethoxysilane

There total 1 articles about Pd-Cl 3-((3,5-bis(phenylsulfanylmethyl)phenoxy)propyltrimethoxysilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

[PdCl(C6H2(CH2SPh)-2,6-(OH)-4)] (1070800-09-7,748150-00-7) + 3-iodopropyltrimethoxysilane (14867-28-8) → Pd-Cl 3-((3,5-bis(phenylsulfanylmethyl)phenoxy)propyltrimethoxysilane (748150-01-8)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; Pd-complex was mixed with 1 equiv. of I-compd. and Cs2CO3 in dry DMF, stirring at 80 °C for 16 h; DMF was distd. off, recrystn. from CH2Cl2/hexane, elem. anal.;

DOI:10.1016/j.jcat.2004.05.015

upstream raw materials:

[PdCl(C₆H₂(CH₂SPh)-2,6-(OH)-4)]

3-iodopropyltrimethoxysilane