7,8-dihydro-N⁶,7-di-p-toluyl-2',3'-O-isopropylidene-8,5'-O-cycloadenosine

Base Information

• Chemical Name: 7,8-dihydro-N⁶,7-di-p-toluyl-2',3'-O-isopropylidene-8,5'-O-cycloadenosine
• CAS No.: 93135-74-1
• Molecular Formula: C₂₉H₂₉N₅O₆
• Molecular Weight: 543.579

Synonyms:7,8-dihydro-N⁶,7-di-p-toluyl-2',3'-O-isopropylidene-8,5'-O-cycloadenosine

Chemical Property of 7,8-dihydro-N⁶,7-di-p-toluyl-2',3'-O-isopropylidene-8,5'-O-cycloadenosine

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Technology Process of 7,8-dihydro-N⁶,7-di-p-toluyl-2',3'-O-isopropylidene-8,5'-O-cycloadenosine

There total 11 articles about 7,8-dihydro-N⁶,7-di-p-toluyl-2',3'-O-isopropylidene-8,5'-O-cycloadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

N6,N6-di-p-toluyl-2',3'-O-isopropylideneadenosine (103062-68-6) → 7,8-dihydro-N6,7-di-p-toluyl-2',3'-O-isopropylidene-8,5'-O-cycloadenosine (93135-74-1)

Guidance literature:

With zinc dibromide; In 1,4-dioxane; Ambient temperature;

Reference yield: 50.0%

2',3'-isopropylidene adenosine (362-75-4) + 4-methyl-benzoyl chloride (874-60-2) → 2',3'-O-isopropylidene-N6,N6,5'-O-tri-p-toluyladenosine (51008-69-6) + N6,5'-O-di-p-toluyl-2',3'-O-isopropylideneadenosine (93135-72-9) + 7,8-dihydro-N6,7-di-p-toluyl-2',3'-O-isopropylidene-8,5'-O-cycloadenosine (93135-74-1) + 7,8-dihydro-2',3'-O-isopropylidene-N6,N6,7-tri-p-toluyl-8,5'-O-cycloadenosine (93135-61-6)

Guidance literature:

With pyridine; In dichloromethane; Ambient temperature; var. reag.: Et₃N;

Reference yield: 34.0%

2',3'-isopropylidene adenosine (362-75-4) + 4-methyl-benzoyl chloride (874-60-2) → 2',3'-O-isopropylidene-N6,N6,5'-O-tri-p-toluyladenosine (51008-69-6) + 4-cyano-1-(2,3-O-isopropylidene-5-O-p-toluyl-β-D-ribofuranosyl)-5-(p-toluylamino)imidazole (93135-75-2) + 7,8-dihydro-N6,7-di-p-toluyl-2',3'-O-isopropylidene-8,5'-O-cycloadenosine (93135-74-1) + 7,8-dihydro-2',3'-O-isopropylidene-N6,N6,7-tri-p-toluyl-8,5'-O-cycloadenosine (93135-61-6)

Guidance literature:

In dichloromethane; triethylamine; for 24h; Ambient temperature;

DOI:10.1021/jo00200a010

upstream raw materials:

p-methylbenzoic anhydride

2',3'-isopropylidene adenosine

4-methyl-benzoyl chloride

N⁶,N⁶-di-p-toluyl-2',3'-O-isopropylideneadenosine

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