(2S,3S)-3-Methyl-2-(3-tritylsulfanyl-propionylamino)-pentanoic acid phenethyl-amide

Base Information

Chemical Name:(2S,3S)-3-Methyl-2-(3-tritylsulfanyl-propionylamino)-pentanoic acid phenethyl-amide
CAS No.:1026366-79-9
Molecular Formula:C₃₆H₄₀N₂O₂S
Molecular Weight:564.792
Hs Code.:

Synonyms:(2S,3S)-3-Methyl-2-(3-tritylsulfanyl-propionylamino)-pentanoic acid phenethyl-amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S)-3-Methyl-2-(3-tritylsulfanyl-propionylamino)-pentanoic acid phenethyl-amide

Chemical Property:

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Technology Process of (2S,3S)-3-Methyl-2-(3-tritylsulfanyl-propionylamino)-pentanoic acid phenethyl-amide

There total 4 articles about (2S,3S)-3-Methyl-2-(3-tritylsulfanyl-propionylamino)-pentanoic acid phenethyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27144-18-9
3-(tritylthio) propanoic acid

: L-isoleucine-phenethylamide hydrochloride

: 1026366-79-9
(2S,3S)-3-Methyl-2-(3-tritylsulfanyl-propionylamino)-pentanoic acid phenethyl-amide

Guidance literature:: With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; In N,N-dimethyl-formamide;
DOI:10.1021/jm00020a010

Reference yield:

: 13139-16-7
N-(tert-butyloxycarbonyl)-L-isoleucine

: 1026366-79-9
(2S,3S)-3-Methyl-2-(3-tritylsulfanyl-propionylamino)-pentanoic acid phenethyl-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide, 3,4-dihydro-3-hydroxy-4-oxo-1,2,3-benzotriazine, Et₃N / dimethylformamide

2: HCl gas / ethyl acetate

3: 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide, 3,4-dihydro-3-hydroxy-4-oxo-1,2,3-benzotriazine, Et₃N / dimethylformamide

With hydrogenchloride; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm00020a010

Reference yield:

: 64-04-0
phenethylamine

: 1026366-79-9
(2S,3S)-3-Methyl-2-(3-tritylsulfanyl-propionylamino)-pentanoic acid phenethyl-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide, 3,4-dihydro-3-hydroxy-4-oxo-1,2,3-benzotriazine, Et₃N / dimethylformamide

2: HCl gas / ethyl acetate

3: 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide, 3,4-dihydro-3-hydroxy-4-oxo-1,2,3-benzotriazine, Et₃N / dimethylformamide

With hydrogenchloride; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm00020a010