[3-(5-Benzyloxy-2-methyl-cyclohex-1-enyl)-propylidene]-triphenyl-λ⁵-phosphane

Base Information

Chemical Name:[3-(5-Benzyloxy-2-methyl-cyclohex-1-enyl)-propylidene]-triphenyl-λ⁵-phosphane
CAS No.:85221-03-0
Molecular Formula:C₃₅H₃₇OP
Molecular Weight:504.652
Hs Code.:

[3-(5-Benzyloxy-2-methyl-cyclohex-1-enyl)-propylidene]-triphenyl-λ<sup>5</sup>-phosphane

Synonyms:[3-(5-Benzyloxy-2-methyl-cyclohex-1-enyl)-propylidene]-triphenyl-λ⁵-phosphane

Suppliers and Price of [3-(5-Benzyloxy-2-methyl-cyclohex-1-enyl)-propylidene]-triphenyl-λ⁵-phosphane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [3-(5-Benzyloxy-2-methyl-cyclohex-1-enyl)-propylidene]-triphenyl-λ⁵-phosphane

Chemical Property:

Purity/Quality:

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Technology Process of [3-(5-Benzyloxy-2-methyl-cyclohex-1-enyl)-propylidene]-triphenyl-λ⁵-phosphane

There total 6 articles about [3-(5-Benzyloxy-2-methyl-cyclohex-1-enyl)-propylidene]-triphenyl-λ⁵-phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85221-02-9
[3-(5-Benzyloxy-2-methyl-cyclohex-1-enyl)-propyl]-triphenyl-phosphonium; bromide

: 85221-03-0
[3-(5-Benzyloxy-2-methyl-cyclohex-1-enyl)-propylidene]-triphenyl-λ⁵-phosphane

Guidance literature:: With phenyllithium; In tetrahydrofuran; diethyl ether; Ambient temperature;
DOI:10.1021/ja00346a073

Reference yield:

: 73658-27-2
4-Benzyloxy-1-methyl-2-methylene-cyclohexanol

: 85221-03-0
[3-(5-Benzyloxy-2-methyl-cyclohex-1-enyl)-propylidene]-triphenyl-λ⁵-phosphane

Guidance literature:: Multi-step reaction with 6 steps

1: 62 percent / Hg(OAc)2 / Heating

2: 92 percent / LiAlH₄ / diethyl ether / 0 °C

3: pyridine / 0 °C

4: LiBr / acetone / Heating

5: benzene / Heating

6: C₆H₅Li / diethyl ether; tetrahydrofuran / Ambient temperature

With pyridine; lithium aluminium tetrahydride; mercury(II) diacetate; phenyllithium; lithium bromide; In tetrahydrofuran; diethyl ether; acetone; benzene;
DOI:10.1021/ja00346a073

Reference yield:

: 85221-01-8
3-(5-Benzyloxy-2-methyl-cyclohex-1-enyl)-propan-1-ol

: 85221-03-0
[3-(5-Benzyloxy-2-methyl-cyclohex-1-enyl)-propylidene]-triphenyl-λ⁵-phosphane

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 0 °C

2: LiBr / acetone / Heating

3: benzene / Heating

4: C₆H₅Li / diethyl ether; tetrahydrofuran / Ambient temperature

With pyridine; phenyllithium; lithium bromide; In tetrahydrofuran; diethyl ether; acetone; benzene;
DOI:10.1021/ja00346a073