2N(CH₂CH₂CH₂CH₃)4⁽¹⁺⁾*[Pd(C₆Cl₅)4]^(2-)=[N(CH₂CH₂CH₂CH₃)4]2[Pd(C₆Cl₅)4]

Base Information

• Chemical Name: 2N(CH₂CH₂CH₂CH₃)4⁽¹⁺⁾*[Pd(C₆Cl₅)4]^(2-)=[N(CH₂CH₂CH₂CH₃)4]2[Pd(C₆Cl₅)4]
• CAS No.: 86391-95-9
• Molecular Formula: 2C₁₆H₃₆N*C₂₄Cl₂₀Pd
• Molecular Weight: 1588.68

Synonyms:2N(CH₂CH₂CH₂CH₃)4⁽¹⁺⁾*[Pd(C₆Cl₅)4]^(2-)=[N(CH₂CH₂CH₂CH₃)4]2[Pd(C₆Cl₅)4]

Chemical Property of 2N(CH₂CH₂CH₂CH₃)4⁽¹⁺⁾*[Pd(C₆Cl₅)4]^(2-)=[N(CH₂CH₂CH₂CH₃)4]2[Pd(C₆Cl₅)4]

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Technology Process of 2N(CH₂CH₂CH₂CH₃)4⁽¹⁺⁾*[Pd(C₆Cl₅)4]^(2-)=[N(CH₂CH₂CH₂CH₃)4]2[Pd(C₆Cl₅)4]

There total 3 articles about 2N(CH₂CH₂CH₂CH₃)4⁽¹⁺⁾*[Pd(C₆Cl₅)4]^(2-)=[N(CH₂CH₂CH₂CH₃)4]2[Pd(C₆Cl₅)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

(NBu4)2{Pd2(μ-Br)2Br4} + tetrabutylammomium bromide (1643-19-2) + pentachlorophenyllithium (6782-80-5) → (NBu4)2{palladium(μ-Br)bis(pentachlorophenyl)}2 (86392-02-1) + 2N(CH2CH2CH2CH3)4(1+)*[Pd(C6Cl5)4](2-)=[N(CH2CH2CH2CH3)4]2[Pd(C6Cl5)4] (86391-95-9)

Guidance literature:

In diethyl ether; to soln. of C6Cl5Li in Et2O added Pd complex at -78 °C, stirred for 17 h at room temp.; moist air passed through system, evapd., extd. with acetone, filtered, concd., crystd. by addn. of EtOH (yield of monomer complex improved by addn. of NBu4Br);soln. concd.,washed with hexane, dimer pptd. by addn. ofH2O, recrystd. from CH2Cl2/2-propanol;

DOI:10.1021/om50004a023

Reference yield: 60.0%

(NBu4)2{palladium(μ-Br)bis(pentachlorophenyl)}2 (86392-02-1) + tetrabutylammomium bromide (1643-19-2) + pentachlorophenyllithium (6782-80-5) → 2N(CH2CH2CH2CH3)4(1+)*[Pd(C6Cl5)4](2-)=[N(CH2CH2CH2CH3)4]2[Pd(C6Cl5)4] (86391-95-9)

Guidance literature:

In diethyl ether; to soln. of C6Cl5Li in Et2O added Pd complex at -78 °C, stirred for 17 h at room temp.; moist air passed through system, evapd., extd. with acetone, filtered, concd., crystd. by addn. of EtOH (yield of Pd complex improved by addn. of NBu4Br); elem. anal.;

DOI:10.1021/om50004a023

Reference yield:

hexachlorobenzene (118-74-1,67471-27-6) → 2N(CH2CH2CH2CH3)4(1+)*[Pd(C6Cl5)4](2-)=[N(CH2CH2CH2CH3)4]2[Pd(C6Cl5)4] (86391-95-9)

Guidance literature:

Multi-step reaction with 2 steps

1: Mg; benzyl bromide / benzene; tetrahydrofuran

2: diethyl ether

With Mg; benzyl bromide; In tetrahydrofuran; diethyl ether; benzene;

DOI:10.1021/om50004a023

upstream raw materials:

(NBu4)2{palladium(μ-Br)bis(pentachlorophenyl)}2

tetrabutylammomium bromide

pentachlorophenyllithium

hexachlorobenzene

Downstream raw materials:

Pd(C₆Cl₅)2(P(C₆H₅)3)2

2N(CH₂CH₂CH₂CH₃)4⁽¹⁺⁾*2Pd⁽²⁺⁾*4(C₆Cl₅)^(1-)*2(SCN)^(1-)=[N(CH₂CH₂CH₂CH₃)4]2[Pd₂(C₆Cl₅)4(SCN)2]

[NBu4]2[[Pd(C6Cl5)2]2(μ-I)2]

Pd(C₆Cl₅)2(C₅H₅N)2

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