3,5-bis(10-undecenyloxy)-4-dodecyloxybenzoic acid ethyl ester

Base Information

Chemical Name:3,5-bis(10-undecenyloxy)-4-dodecyloxybenzoic acid ethyl ester
CAS No.:887914-48-9
Molecular Formula:C₄₃H₇₄O₅
Molecular Weight:671.058
Hs Code.:

Synonyms:3,5-bis(10-undecenyloxy)-4-dodecyloxybenzoic acid ethyl ester

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Chemical Property of 3,5-bis(10-undecenyloxy)-4-dodecyloxybenzoic acid ethyl ester

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Technology Process of 3,5-bis(10-undecenyloxy)-4-dodecyloxybenzoic acid ethyl ester

There total 6 articles about 3,5-bis(10-undecenyloxy)-4-dodecyloxybenzoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 887914-40-1
ethyl 4-(dodecyloxy)-3,5-dihydroxybenzoate

: 7766-49-6
1-iodo-10-undecene

: 887914-48-9
3,5-bis(10-undecenyloxy)-4-dodecyloxybenzoic acid ethyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 3h;
DOI:10.1021/ja0606935

Reference yield:

: 887914-38-7
ethyl 3,5-bis[(tert-butyldimethylsilyl)oxy]-4-hydroxybenzoate

: 887914-48-9
3,5-bis(10-undecenyloxy)-4-dodecyloxybenzoic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / triphenylphosphine; diethyl azodicarboxylate / toluene / 10 h / 20 °C

2: 100 percent / tetrabutylammonium fluoride / CH₂Cl₂ / 10 h / 20 °C

3: 78 percent / K₂CO₃ / dimethylformamide / 3 h / 70 °C

With tetrabutyl ammonium fluoride; potassium carbonate; triphenylphosphine; diethylazodicarboxylate; In dichloromethane; N,N-dimethyl-formamide; toluene; 1: Mitsunobu reaction;
DOI:10.1021/ja0606935

Reference yield:

: 887914-39-8
ethyl 3,5-bis[(tert-butyldimethylsilyl)oxy]-4-dodecyloxybenzoate

: 887914-48-9
3,5-bis(10-undecenyloxy)-4-dodecyloxybenzoic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / tetrabutylammonium fluoride / CH₂Cl₂ / 10 h / 20 °C

2: 78 percent / K₂CO₃ / dimethylformamide / 3 h / 70 °C

With tetrabutyl ammonium fluoride; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja0606935