cyclohexyl(6-(4-methylthiophenyl)-2H-benzo[d]1,3-dioxolan-5-yl)methan-1-ol

Base Information

Chemical Name:cyclohexyl(6-(4-methylthiophenyl)-2H-benzo[d]1,3-dioxolan-5-yl)methan-1-ol
CAS No.:445039-75-8
Molecular Formula:C₂₁H₂₄O₃S
Molecular Weight:356.486
Hs Code.:

Synonyms:cyclohexyl(6-(4-methylthiophenyl)-2H-benzo[d]1,3-dioxolan-5-yl)methan-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cyclohexyl(6-(4-methylthiophenyl)-2H-benzo[d]1,3-dioxolan-5-yl)methan-1-ol

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Technology Process of cyclohexyl(6-(4-methylthiophenyl)-2H-benzo[d]1,3-dioxolan-5-yl)methan-1-ol

There total 4 articles about cyclohexyl(6-(4-methylthiophenyl)-2H-benzo[d]1,3-dioxolan-5-yl)methan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: ammonium chloride

: 931-50-0
cyclohexylmagnesium bromide

: 445039-73-6
6-(4-methylthiophenyl)-2H-benzo[d]1,3-dioxolane-5-carbaldehyde

: 445039-75-8
cyclohexyl(6-(4-methylthiophenyl)-2H-benzo[d]1,3-dioxolan-5-yl)methan-1-ol

Guidance literature:: In tetrahydrofuran; hexane; ethyl acetate;

Reference yield: 93.0%

: 931-50-0
cyclohexylmagnesium bromide

: 445039-73-6
6-(4-methylthiophenyl)-2H-benzo[d]1,3-dioxolane-5-carbaldehyde

: 445039-75-8
cyclohexyl(6-(4-methylthiophenyl)-2H-benzo[d]1,3-dioxolan-5-yl)methan-1-ol

Guidance literature:: In tetrahydrofuran; at 0 - 20 ℃; for 2.16667h;
DOI:10.1021/jm030268b

Reference yield:

: 120-57-0,30024-74-9
piperonal

: 445039-75-8
cyclohexyl(6-(4-methylthiophenyl)-2H-benzo[d]1,3-dioxolan-5-yl)methan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / bromine; acetic acid; iodine / CS₂ / 20 °C

2: 88 percent / sodium carbonate; tetrakis(triphenylphosphine)palladium / ethanol / Heating

3: 93 percent / tetrahydrofuran / 2.17 h / 0 - 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; bromine; iodine; sodium carbonate; acetic acid; In tetrahydrofuran; carbon disulfide; ethanol; 2: Suzuki coupling / 3: Grignard reaction;
DOI:10.1021/jm030268b