3-Iodophthalonitrile

Base Information

Chemical Name:3-Iodophthalonitrile
CAS No.:76241-81-1
Molecular Formula:C₈H₃IN₂
Molecular Weight:254.03
Hs Code.:
European Community (EC) Number:870-843-4
Nikkaji Number:J949.335B

Synonyms:3-Iodophthalonitrile;76241-81-1;3-IODOBENZENE-1,2-DICARBONITRILE;iodophthalonitrile;SCHEMBL3957849;EN300-23906420

Suppliers and Price of 3-Iodophthalonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3-Iodophthalonitrile

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:253.93410
Heavy Atom Count:11
Complexity:231

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=C(C(=C1)I)C#N)C#N

Technology Process of 3-Iodophthalonitrile

There total 4 articles about 3-Iodophthalonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₆N₄Zn

: 76241-81-1
1,2-dicyano-3-iodobenzene

Guidance literature:: With iodine; In tetrahydrofuran; at 0 ℃; for 2h; Inert atmosphere; Flow reactor;
DOI:10.1055/s-0036-1588837

Reference yield:

: 91-15-6
phthalonitrile

: 76241-81-1
1,2-dicyano-3-iodobenzene

Guidance literature:: phthalonitrile; With 2,2,6,6-tetramethylpiperidinyl-lithium; In tetrahydrofuran; hexane; at -78 ℃;

With iodine; In tetrahydrofuran; hexane; at -78 - 20 ℃; Further stages.;
DOI:10.1021/jo026178g

Reference yield:

: 51762-67-5
3-nitrobenzene-1,2-dicarbonitrile

: 76241-81-1
1,2-dicyano-3-iodobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / H₂ / 5percent Pd/BaSO₄ poisoned with thiourea / dioxane; ethanol / 1 h / 1551.4 Torr / Ambient temperature

2: 1.) NaNO₂, conc. HCl, 2.) KI / 1.) H₂O, 5 deg C, 1.5 h, 2.) H₂O, 0.5 h

With hydrogenchloride; hydrogen; potassium iodide; sodium nitrite; Pd-BaSO₄; BaSO₄ poisoned with thiourea; In 1,4-dioxane; ethanol;