C₁₅H₂₂NO₃P

Base Information

Chemical Name:C₁₅H₂₂NO₃P
CAS No.:1001095-86-8
Molecular Formula:C₁₅H₂₂NO₃P
Molecular Weight:295.318
Hs Code.:

C<sub>15</sub>H<sub>22</sub>NO<sub>3</sub>P

Synonyms:C₁₅H₂₂NO₃P

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Chemical Property of C₁₅H₂₂NO₃P

Chemical Property:

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Technology Process of C₁₅H₂₂NO₃P

There total 7 articles about C₁₅H₂₂NO₃P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1001095-85-7
C₂₃H₂₈NO₅P

: 1001095-86-8
C₁₅H₂₂NO₃P

Guidance literature:: With dimethylsulfide; trifluoroacetic acid; at 20 ℃;

Reference yield:

: 877068-76-3
diethyl (1S,2S)-1-amino-2-vinyl-cyclopropane-1-phosphonate

: 1001095-86-8
C₁₅H₂₂NO₃P

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydrogencarbonate / dichloromethane; water / 20 °C

2.1: pyridine; sodium iodide / 105 °C

3.1: oxalyl dichloride; N,N-dimethyl-formamide / toluene / 0 - 20 °C

4.1: lithium tri-t-butoxyaluminum hydride / tetrahydrofuran / -40 °C

5.1: N-ethyl-N,N-diisopropylamine / dichloromethane

6.1: 20 - 40 °C

7.1: trimethylsilyl iodide / acetonitrile

7.2: 0 - 20 °C

With pyridine; oxalyl dichloride; trimethylsilyl iodide; sodium hydrogencarbonate; lithium tri-t-butoxyaluminum hydride; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; sodium iodide; In tetrahydrofuran; dichloromethane; water; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2011.04.125

Reference yield:

: 877068-79-6
(1-benzyloxycarbonylamino-2-vinyl-cyclopropyl)-phosphonic acid monoethyl ester

: 1001095-86-8
C₁₅H₂₂NO₃P

Guidance literature:: Multi-step reaction with 5 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / toluene / 0 - 20 °C

2.1: lithium tri-t-butoxyaluminum hydride / tetrahydrofuran / -40 °C

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane

4.1: 20 - 40 °C

5.1: trimethylsilyl iodide / acetonitrile

5.2: 0 - 20 °C

With oxalyl dichloride; trimethylsilyl iodide; lithium tri-t-butoxyaluminum hydride; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; toluene; acetonitrile;
DOI:10.1016/j.bmcl.2011.04.125