Re(CNC(CH₃)3)3(P(C₆H₁₁)3)2H₂⁽¹⁺⁾*BF₄^(1-)=[Re(CNC(CH₃)3)3(P(C₆H₁₁)3)2H₂]BF₄

Base Information

• Chemical Name: Re(CNC(CH₃)3)3(P(C₆H₁₁)3)2H₂⁽¹⁺⁾*BF₄^(1-)=[Re(CNC(CH₃)3)3(P(C₆H₁₁)3)2H₂]BF₄
• CAS No.: 183674-90-0
• Molecular Formula: BF₄*C₅₁H₉₅N₃P₂Re
• Molecular Weight: 1085.29
• Mol file: 183674-90-0.mol

Synonyms:Re(CNC(CH₃)3)3(P(C₆H₁₁)3)2H₂⁽¹⁺⁾*BF₄^(1-)=[Re(CNC(CH₃)3)3(P(C₆H₁₁)3)2H₂]BF₄

Chemical Property of Re(CNC(CH₃)3)3(P(C₆H₁₁)3)2H₂⁽¹⁺⁾*BF₄^(1-)=[Re(CNC(CH₃)3)3(P(C₆H₁₁)3)2H₂]BF₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Re(CNC(CH₃)3)3(P(C₆H₁₁)3)2H₂⁽¹⁺⁾*BF₄^(1-)=[Re(CNC(CH₃)3)3(P(C₆H₁₁)3)2H₂]BF₄

There total 1 articles about Re(CNC(CH₃)3)3(P(C₆H₁₁)3)2H₂⁽¹⁺⁾*BF₄^(1-)=[Re(CNC(CH₃)3)3(P(C₆H₁₁)3)2H₂]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

tetrafluoroboric acid diethyl ether (67969-82-8) + Re(CNC(CH3)3)3(P(C6H11)3)2H (183674-83-1) → Re(CNC(CH3)3)3(P(C6H11)3)2H2(1+)*BF4(1-)=[Re(CNC(CH3)3)3(P(C6H11)3)2H2]BF4 (183674-90-0)

Guidance literature:

In diethyl ether; (Ar); filtration, drying in H2;

DOI:10.1021/ja961994p

Reference yield:

Re(CNC(CH3)3)3(P(C6H11)3)2H2(1+)*BF4(1-)=[Re(CNC(CH3)3)3(P(C6H11)3)2H2]BF4 (183674-90-0) → Re(CNC(CH3)3)3(P(C6H11)3)2(1+)*BF4(1-)=[Re(CNC(CH3)3)3(P(C6H11)3)2]BF4 (183675-01-6)

Guidance literature:

exposition to dynamic vacuum (24 h, 23°C); recrystn. (THF), elem. anal.;

DOI:10.1021/ja961994p

upstream raw materials:

tetrafluoroboric acid diethyl ether

Re(CNC(CH₃)3)3(P(C₆H₁₁)3)2H

Downstream raw materials:

Re(CNC(CH₃)3)3(P(C₆H₁₁)3)2⁽¹⁺⁾*BF₄^(1-)=[Re(CNC(CH₃)3)3(P(C₆H₁₁)3)2]BF₄