2N-benzyloxy-3,4,5-tris(benzyloxy)-6-benzyloxymethyl-(3S,4S,5R,6S)-tetrahydro-2H-pyran-2-imine

Base Information

Chemical Name:2N-benzyloxy-3,4,5-tris(benzyloxy)-6-benzyloxymethyl-(3S,4S,5R,6S)-tetrahydro-2H-pyran-2-imine
CAS No.:270062-28-7
Molecular Formula:C₄₁H₄₁NO₆
Molecular Weight:643.78
Hs Code.:

Synonyms:2N-benzyloxy-3,4,5-tris(benzyloxy)-6-benzyloxymethyl-(3S,4S,5R,6S)-tetrahydro-2H-pyran-2-imine

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Chemical Property of 2N-benzyloxy-3,4,5-tris(benzyloxy)-6-benzyloxymethyl-(3S,4S,5R,6S)-tetrahydro-2H-pyran-2-imine

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Technology Process of 2N-benzyloxy-3,4,5-tris(benzyloxy)-6-benzyloxymethyl-(3S,4S,5R,6S)-tetrahydro-2H-pyran-2-imine

There total 3 articles about 2N-benzyloxy-3,4,5-tris(benzyloxy)-6-benzyloxymethyl-(3S,4S,5R,6S)-tetrahydro-2H-pyran-2-imine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 270062-23-2
1N-benzyloxy-2,3,4,6-tetrakis(benzyloxy)-5-hydroxy-(2S,3S,4R,5R)-hexanamide

: 270062-28-7
2N-benzyloxy-3,4,5-tris(benzyloxy)-6-benzyloxymethyl-(3S,4S,5R,6S)-tetrahydro-2H-pyran-2-imine

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃; for 0.166667h;
DOI:10.1021/ja992808t

Reference yield:

: 622-33-3
N-benzyloxyamine

: 270062-28-7
2N-benzyloxy-3,4,5-tris(benzyloxy)-6-benzyloxymethyl-(3S,4S,5R,6S)-tetrahydro-2H-pyran-2-imine

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / trimethylaluminum / CH₂Cl₂ / 1 h / 20 °C

2: 91 percent / PPh₃; DEAD / tetrahydrofuran / 0.17 h / 20 °C

With trimethylaluminum; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; 1: Alkoxyamination / 2: Cyclization;
DOI:10.1021/ja992808t

Reference yield:

: 82598-88-7
2,3,4,6-tetra-O-benzyl-D-mannono-1,5-lactone

: 270062-28-7
2N-benzyloxy-3,4,5-tris(benzyloxy)-6-benzyloxymethyl-(3S,4S,5R,6S)-tetrahydro-2H-pyran-2-imine

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / trimethylaluminum / CH₂Cl₂ / 1 h / 20 °C

2: 91 percent / PPh₃; DEAD / tetrahydrofuran / 0.17 h / 20 °C

With trimethylaluminum; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; 1: Alkoxyamination / 2: Cyclization;
DOI:10.1021/ja992808t