benzyl N-[(6-[(methylamino)carbonyl]-2-pyridylmethyl)amino]carbothioyl carbamate

Base Information

Chemical Name:benzyl N-[(6-[(methylamino)carbonyl]-2-pyridylmethyl)amino]carbothioyl carbamate
CAS No.:944150-43-0
Molecular Formula:C₁₇H₁₈N₄O₃S
Molecular Weight:358.421
Hs Code.:

Synonyms:benzyl N-[(6-[(methylamino)carbonyl]-2-pyridylmethyl)amino]carbothioyl carbamate

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Chemical Property of benzyl N-[(6-[(methylamino)carbonyl]-2-pyridylmethyl)amino]carbothioyl carbamate

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Technology Process of benzyl N-[(6-[(methylamino)carbonyl]-2-pyridylmethyl)amino]carbothioyl carbamate

There total 2 articles about benzyl N-[(6-[(methylamino)carbonyl]-2-pyridylmethyl)amino]carbothioyl carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 944150-29-2
6-(aminomethyl)-N²-methylpyridine-2-carboxamide

: 63220-36-0
benzyloxycarbonyl isothiocyanate

: 944150-43-0
benzyl N-[(6-[(methylamino)carbonyl]-2-pyridylmethyl)amino]carbothioyl carbamate

Guidance literature:: In dichloromethane; for 4h;
DOI:10.1039/b700988g

Reference yield:

: 944150-30-5
ethyl 6-((1,3-dioxoisoindolin-2-yl)methyl)picolinate

: 944150-43-0
benzyl N-[(6-[(methylamino)carbonyl]-2-pyridylmethyl)amino]carbothioyl carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 39 percent / H₂O / 18 h

2: 51 percent / CH₂Cl₂ / 4 h

In dichloromethane; water;
DOI:10.1039/b700988g

Reference yield: 40.0%

: 944150-43-0
benzyl N-[(6-[(methylamino)carbonyl]-2-pyridylmethyl)amino]carbothioyl carbamate

: benzyl N-5-[(methylamino)carbonyl]imidazo[1,5-a]pyridin-3-yl-carbamate

Guidance literature:: With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 8h;
DOI:10.1039/b700988g