1-(3-ethoxy-4-methoxybenzyl)-4-(pyridin-2-ylmethyl)piperazinediium

Base Information

• Chemical Name: 1-(3-ethoxy-4-methoxybenzyl)-4-(pyridin-2-ylmethyl)piperazinediium
• CAS No.: 6713-26-4
• Molecular Formula: C20H29N3O2+2
• Molecular Weight: 456.709
• Mol file: 6713-26-4.mol

Synonyms:

Chemical Property of 1-(3-ethoxy-4-methoxybenzyl)-4-(pyridin-2-ylmethyl)piperazinediium

Chemical Property:

• Vapor Pressure: 1.71E-08mmHg at 25°C
• Boiling Point: 455.7°C at 760 mmHg
• Flash Point: 229.4°C

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(3-ethoxy-4-methoxybenzyl)-4-(pyridin-2-ylmethyl)piperazinediium

There total 4 articles about 1-(3-ethoxy-4-methoxybenzyl)-4-(pyridin-2-ylmethyl)piperazinediium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

benzyl-3β-hydroxy-oleanorane-13(18)-en-28-ester → δ-oleanolic acid (6713-26-4)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; at 20 ℃;

DOI:10.1039/c6ob02126c

Reference yield:

benzyl 3β-hydroxyolean-12-en-28-oate → δ-oleanolic acid (6713-26-4)

Guidance literature:

Multi-step reaction with 2 steps

1: proton-exchanged montmorillonite / dichloromethane / 0.67 h / 40 °C

2: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 20 °C

With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; dichloromethane;

DOI:10.1039/c6ob02126c

Reference yield:

Oleanolic acid (508-02-1) → δ-oleanolic acid (6713-26-4)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2: proton-exchanged montmorillonite / dichloromethane / 0.67 h / 40 °C

3: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 20 °C

With palladium 10% on activated carbon; hydrogen; potassium carbonate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1039/c6ob02126c

upstream raw materials:

Oleanolic acid

Downstream raw materials:

28-nor-olean-17-en-3β-ol

olean-13(18)-en-3β-yl acetate