(2S)-N-{4-[3-[2-methoxy-4-((E)-3-oxo-3-[4-(3,4,5-trimethoxybenzoyl)piperazino]-1-propenyl)phenoxy]propoxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal

Base Information

Chemical Name:(2S)-N-{4-[3-[2-methoxy-4-((E)-3-oxo-3-[4-(3,4,5-trimethoxybenzoyl)piperazino]-1-propenyl)phenoxy]propoxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal
CAS No.:1226908-98-0
Molecular Formula:C₄₄H₅₆N₄O₁₂S₂
Molecular Weight:897.08
Hs Code.:

(2S)-N-{4-[3-[2-methoxy-4-((E)-3-oxo-3-[4-(3,4,5-trimethoxybenzoyl)piperazino]-1-propenyl)phenoxy]propoxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal

Synonyms:(2S)-N-{4-[3-[2-methoxy-4-((E)-3-oxo-3-[4-(3,4,5-trimethoxybenzoyl)piperazino]-1-propenyl)phenoxy]propoxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal

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Chemical Property of (2S)-N-{4-[3-[2-methoxy-4-((E)-3-oxo-3-[4-(3,4,5-trimethoxybenzoyl)piperazino]-1-propenyl)phenoxy]propoxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal

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Technology Process of (2S)-N-{4-[3-[2-methoxy-4-((E)-3-oxo-3-[4-(3,4,5-trimethoxybenzoyl)piperazino]-1-propenyl)phenoxy]propoxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal

There total 1 articles about (2S)-N-{4-[3-[2-methoxy-4-((E)-3-oxo-3-[4-(3,4,5-trimethoxybenzoyl)piperazino]-1-propenyl)phenoxy]propoxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1226909-06-3
(E)-3-(4-hydroxy-3-methoxyphenyl)-1-[4-(3,4,5-trimethoxybenzoyl)piperazino]-2-propen-1-one

: 343308-55-4
(2S)-N-[4-(3-bromopropoxy)-5-methoxy-2-nitrobenzoyl]pyrrolidine-2-carboxaldehyde diethyl thioacetal

: 1226908-98-0
(2S)-N-{4-[3-[2-methoxy-4-((E)-3-oxo-3-[4-(3,4,5-trimethoxybenzoyl)piperazino]-1-propenyl)phenoxy]propoxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal

Guidance literature:: With potassium carbonate; In acetonitrile; for 12h; Reflux;
DOI:10.1016/j.ejmech.2010.05.041

Reference yield:

: 1226908-98-0
(2S)-N-{4-[3-[2-methoxy-4-((E)-3-oxo-3-[4-(3,4,5-trimethoxybenzoyl)piperazino]-1-propenyl)phenoxy]propoxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal

: 1226908-99-1
C₄₄H₅₈N₄O₁₀S₂

Guidance literature:: (2S)-N-{4-[3-[2-methoxy-4-((E)-3-oxo-3-[4-(3,4,5-trimethoxybenzoyl)piperazino]-1-propenyl)phenoxy]propoxy]-5-methoxy-2-nitrobenzoyl}pyrrolidine-2-carboxaldehyde diethyl dithioacetal; With tin(II) chloride dihdyrate; In methanol; for 5h; Reflux;

With sodium hydrogencarbonate; In water; pH=8;