3-p-tolylsulphonylpropyl benzenesulphonate

Base Information

• Chemical Name: 3-p-tolylsulphonylpropyl benzenesulphonate
• CAS No.: 82777-13-7
• Molecular Formula: C₁₆H₁₈O₅S₂
• Molecular Weight: 354.448
• Mol file: 82777-13-7.mol

Synonyms:3-p-tolylsulphonylpropyl benzenesulphonate

Chemical Property of 3-p-tolylsulphonylpropyl benzenesulphonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-p-tolylsulphonylpropyl benzenesulphonate

There total 3 articles about 3-p-tolylsulphonylpropyl benzenesulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

Benzenesulfonic acid 3-p-tolylsulfanyl-propyl ester (82777-12-6) → 3-p-tolylsulphonylpropyl benzenesulphonate (82777-13-7)

Guidance literature:

With ammonium molybdate; dihydrogen peroxide; In methanol;

DOI:10.1039/P29820000579

Reference yield:

3-[(4-methylphenyl)sulfanyl]-1-propanol (3147-28-2) → 3-p-tolylsulphonylpropyl benzenesulphonate (82777-13-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 47 percent / pyridine / 0 °C

2: 68 percent / 30 percent aq. hydrogen peroxide, ammonium molybdate / methanol

With ammonium molybdate; dihydrogen peroxide; In pyridine; methanol;

DOI:10.1039/P29820000579

Reference yield:

benzenesulfonyl chloride (98-09-9) → 3-p-tolylsulphonylpropyl benzenesulphonate (82777-13-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 47 percent / pyridine / 0 °C

2: 68 percent / 30 percent aq. hydrogen peroxide, ammonium molybdate / methanol

With ammonium molybdate; dihydrogen peroxide; In pyridine; methanol;

DOI:10.1039/P29820000579

upstream raw materials:

Benzenesulfonic acid 3-p-tolylsulfanyl-propyl ester

3-[(4-methylphenyl)sulfanyl]-1-propanol

benzenesulfonyl chloride

Downstream raw materials:

cyclopropyl p-tolyl sulphone