monic acid, N-p-toluenesulphonylmethyl amide, tris(trimethylsilyl ether)

Base Information

Chemical Name:monic acid, N-p-toluenesulphonylmethyl amide, tris(trimethylsilyl ether)
CAS No.:152366-36-4
Molecular Formula:C₃₄H₆₁NO₈SSi₃
Molecular Weight:728.183
Hs Code.:

Synonyms:monic acid, N-p-toluenesulphonylmethyl amide, tris(trimethylsilyl ether)

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Chemical Property of monic acid, N-p-toluenesulphonylmethyl amide, tris(trimethylsilyl ether)

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Technology Process of monic acid, N-p-toluenesulphonylmethyl amide, tris(trimethylsilyl ether)

There total 4 articles about monic acid, N-p-toluenesulphonylmethyl amide, tris(trimethylsilyl ether) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 824-79-3
sodium 4-methylbenzenesulfinate

: Trimethyl-[((E)-3-methyl-4-{(2S,3S,4R,5S)-5-[(2S,3S)-3-((1R,2S)-1-methyl-2-trimethylsilanyloxy-propyl)-oxiranylmethyl]-3,4-bis-trimethylsilanyloxy-tetrahydro-pyran-2-yl}-but-2-enoylamino)-methyl]-ammonium; iodide

: 152366-36-4
monic acid, N-p-toluenesulphonylmethyl amide, tris(trimethylsilyl ether)

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 18h;
DOI:10.7164/antibiotics.48.1336

Reference yield:

: 66262-68-8,66290-01-5,70470-39-2
monic acid A

: 152366-36-4
monic acid, N-p-toluenesulphonylmethyl amide, tris(trimethylsilyl ether)

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) isobutyl chloroformate, triethylamine, ammonia, 2.) triethylamine, N,N-dimethylaminopyridine / 1.) THF, 0 deg C_. 0.75 h, 2.) 20 deg C, 1.5 h

2: tetrahydrofuran / 1.5 h / 20 °C

3: triethylamine / tetrahydrofuran / 1 h / 20 °C

4: 85 percent / triethylamine / dimethylformamide / 18 h / 20 °C

With dmap; ammonia; triethylamine; isobutyl chloroformate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.7164/antibiotics.48.1336

Reference yield:

: 133674-54-1
monic acid, tris(trimethylsilyl ether)

: 152366-36-4
monic acid, N-p-toluenesulphonylmethyl amide, tris(trimethylsilyl ether)

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 1.5 h / 20 °C

2: triethylamine / tetrahydrofuran / 1 h / 20 °C

3: 85 percent / triethylamine / dimethylformamide / 18 h / 20 °C

With triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.7164/antibiotics.48.1336