4-methoxy-1,2-benzenedithiol

Base Information

Chemical Name:4-methoxy-1,2-benzenedithiol
CAS No.:72546-17-9
Molecular Formula:C₇H₈OS₂
Molecular Weight:172.272
Hs Code.:

Synonyms:4-methoxy-1,2-benzenedithiol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methoxy-1,2-benzenedithiol

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Technology Process of 4-methoxy-1,2-benzenedithiol

There total 7 articles about 4-methoxy-1,2-benzenedithiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 696-63-9
4-Methoxybenzenethiol

: 72546-17-9
4-methoxy-1,2-benzenedithiol

Guidance literature:: 4-Methoxybenzenethiol; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In hexane; at 0 ℃; for 24h; Inert atmosphere; Schlenk technique;

With sulfur; for 12h; Inert atmosphere; Schlenk technique;

With lithium aluminium tetrahydride; for 12h; Reflux; Inert atmosphere; Schlenk technique;
DOI:10.1002/ejic.202000851

Reference yield:

: 128864-24-4
2-(5-Methoxy-benzo[1,3]dithiol-2-ylidene)-malonic acid diethyl ester

: 72546-17-9
4-methoxy-1,2-benzenedithiol

Guidance literature:: With sulfuric acid; zinc diacetate; ethylenediamine; In isopropyl alcohol; for 168h; Yield given; Heating;
DOI:10.1021/jm00031a005