N,N-diallylmesitylsulfonamide

Base Information

Chemical Name:N,N-diallylmesitylsulfonamide
CAS No.:330467-21-5
Molecular Formula:C₁₅H₂₁NO₂S
Molecular Weight:279.403
Hs Code.:

Synonyms:N,N-diallylmesitylsulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-diallylmesitylsulfonamide

Chemical Property:

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Technology Process of N,N-diallylmesitylsulfonamide

There total 1 articles about N,N-diallylmesitylsulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 773-64-8
2-mesitylenesulphonyl chloride

: 124-02-7
diallylamine

: 330467-21-5
N,N-diallylmesitylsulfonamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.tet.2005.01.048

Reference yield: 57.0%

: 330467-21-5
N,N-diallylmesitylsulfonamide

: 766-08-5,146088-00-8
methylphenylsilane

: 849936-05-6
(N-mesitylsulfonyl)-piperidinyl-3-methyl(phenyl)silylmethane

Guidance literature:: With (pentachlorocyclopentadienyl)2Lu(CH₃)*THF; In benzene-d6; at 50 ℃; for 120h;
DOI:10.1016/j.tet.2005.01.048

Reference yield:

: 330467-21-5
N,N-diallylmesitylsulfonamide

: (N-methylsulfonyl)-piperidinyl-3-methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / (pentachlorocyclopentadienyl)2Lu(CH₃)*THF / benzene-d6 / 120 h / 50 °C

2: 63 percent / KH; cumene hydroperoxide; tetrabutylammonium fluoride / 1-methyl-pyrrolidin-2-one / 12 h / 20 °C

With Cumene hydroperoxide; (pentachlorocyclopentadienyl)2Lu(CH₃)*THF; tetrabutyl ammonium fluoride; potassium hydride; In 1-methyl-pyrrolidin-2-one; benzene-d6;
DOI:10.1016/j.tet.2005.01.048