7-(benzyloxycarbonylamino)-N,N′,N′′-tris(tert-butoxycarbonyl)adamantane-1,3,5-triethanamine

Base Information

• Chemical Name: 7-(benzyloxycarbonylamino)-N,N′,N′′-tris(tert-butoxycarbonyl)adamantane-1,3,5-triethanamine
• CAS No.: 1448150-58-0
• Molecular Formula: C₃₉H₆₂N₄O₈
• Molecular Weight: 714.943

Synonyms:7-(benzyloxycarbonylamino)-N,N′,N′′-tris(tert-butoxycarbonyl)adamantane-1,3,5-triethanamine

Chemical Property of 7-(benzyloxycarbonylamino)-N,N′,N′′-tris(tert-butoxycarbonyl)adamantane-1,3,5-triethanamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of 7-(benzyloxycarbonylamino)-N,N′,N′′-tris(tert-butoxycarbonyl)adamantane-1,3,5-triethanamine

There total 2 articles about 7-(benzyloxycarbonylamino)-N,N′,N′′-tris(tert-butoxycarbonyl)adamantane-1,3,5-triethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C27H35NO8 (1351865-49-0) → 7-(benzyloxycarbonylamino)-N,N′,N′′-tris(tert-butoxycarbonyl)adamantane-1,3,5-triethanamine (1448150-58-0)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine; diphenyl phosphoryl azide / dichloromethane / 8 h / 20 °C

2: 24 h / Reflux; Inert atmosphere

With diphenyl phosphoryl azide; triethylamine; In dichloromethane; 2: |Curtius Rearrangement;

DOI:10.1055/s-0033-1338470

Reference yield:

C27H32N10O5 + tert-butyl alcohol (75-65-0) → 7-(benzyloxycarbonylamino)-N,N′,N′′-tris(tert-butoxycarbonyl)adamantane-1,3,5-triethanamine (1448150-58-0)

Guidance literature:

for 24h; Reflux; Inert atmosphere;

DOI:10.1055/s-0033-1338470

Reference yield: 99.0%

7-(benzyloxycarbonylamino)-N,N′,N′′-tris(tert-butoxycarbonyl)adamantane-1,3,5-triethanamine (1448150-58-0) → 7-(benzyloxycarbonylamino)adamantane-1,3,5-triethanamine (1448150-59-1)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1055/s-0033-1338470

upstream raw materials:

C₂₇H₃₅NO₈

tert-butyl alcohol

Downstream raw materials:

7-(benzyloxycarbonylamino)adamantane-1,3,5-triethanamine

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