Ethyl 4-(4-bromo-2-formylphenoxy)-2-butenoate

Base Information

Chemical Name:Ethyl 4-(4-bromo-2-formylphenoxy)-2-butenoate
CAS No.:478064-32-3
Molecular Formula:C₁₃H₁₃BrO₄
Molecular Weight:313.148
Hs Code.:
DSSTox Substance ID:DTXSID101250572

Synonyms:DTXSID101250572;Ethyl 4-(4-bromo-2-formylphenoxy)-2-butenoate;478064-32-3

Suppliers and Price of Ethyl 4-(4-bromo-2-formylphenoxy)-2-butenoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 0 raw suppliers

Chemical Property of Ethyl 4-(4-bromo-2-formylphenoxy)-2-butenoate

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:311.99972
Heavy Atom Count:18
Complexity:303

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOC(=O)C=CCOC1=C(C=C(C=C1)Br)C=O

Technology Process of Ethyl 4-(4-bromo-2-formylphenoxy)-2-butenoate

There total 2 articles about Ethyl 4-(4-bromo-2-formylphenoxy)-2-butenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 6065-32-3
4-bromocrotonic ethyl ester

: 1761-61-1
5-bromosalicyclaldehyde

: 478064-32-3
C₁₃H₁₃BrO₄

Guidance literature:: 5-bromosalicyclaldehyde; With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 0.333333h;

4-bromocrotonic ethyl ester; In N,N-dimethyl-formamide; Cooling with ice;
DOI:10.1039/c0cc01967d

Reference yield:

: C₁₃H₁₅BrO₄

: 478064-32-3
C₁₃H₁₃BrO₄

Guidance literature:: With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; In dimethyl sulfoxide; ethyl acetate; at 0 - 20 ℃; Inert atmosphere;
DOI:10.14233/ajchem.2019.21524