N,N'-Dibenzyl-(5R,6R)-5,6-cyclohexenyl-(2R,9R)-2,9-diphenyl-14,15-naphtho-4,7-diaza-1,10,13,16-tetraoxaoctadecane

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Chemical Name:N,N'-Dibenzyl-(5R,6R)-5,6-cyclohexenyl-(2R,9R)-2,9-diphenyl-14,15-naphtho-4,7-diaza-1,10,13,16-tetraoxaoctadecane
CAS No.:1415402-93-5
Molecular Formula:C₅₀H₅₄N₂O₄
Molecular Weight:746.99
Hs Code.:

Synonyms:N,N'-Dibenzyl-(5R,6R)-5,6-cyclohexenyl-(2R,9R)-2,9-diphenyl-14,15-naphtho-4,7-diaza-1,10,13,16-tetraoxaoctadecane

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Chemical Property of N,N'-Dibenzyl-(5R,6R)-5,6-cyclohexenyl-(2R,9R)-2,9-diphenyl-14,15-naphtho-4,7-diaza-1,10,13,16-tetraoxaoctadecane

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Technology Process of N,N'-Dibenzyl-(5R,6R)-5,6-cyclohexenyl-(2R,9R)-2,9-diphenyl-14,15-naphtho-4,7-diaza-1,10,13,16-tetraoxaoctadecane

There total 3 articles about N,N'-Dibenzyl-(5R,6R)-5,6-cyclohexenyl-(2R,9R)-2,9-diphenyl-14,15-naphtho-4,7-diaza-1,10,13,16-tetraoxaoctadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.65%

: 2,3-bis[2-(p-tolylsulphonyl)ethoxy]naphthalene

: 208037-05-2
(1R,2R)-N,N'-dibenzyl-bis[(R)-2-hydroxy(2-phenyl)ethyl]-1,2-diaminocyclohexane

: 1415402-93-5
N,N'-Dibenzyl-(5R,6R)-5,6-cyclohexenyl-(2R,9R)-2,9-diphenyl-14,15-naphtho-4,7-diaza-1,10,13,16-tetraoxaoctadecane

Guidance literature:: (1R,2R)-N,N'-dibenzyl-bis[(R)-2-hydroxy(2-phenyl)ethyl]-1,2-diaminocyclohexane; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 2h; Reflux; Inert atmosphere;

2,3-bis[2-(p-tolylsulphonyl)ethoxy]naphthalene; In tetrahydrofuran; mineral oil; at 0 ℃; for 96h; Reflux;
DOI:10.1016/j.tet.2012.10.020

Reference yield:

: 65838-10-0,135613-88-6,143443-23-6,191480-61-2
(1R,2R)-N,N'-dibenzylcyclohexane-1,2-diamine

: 1415402-93-5
N,N'-Dibenzyl-(5R,6R)-5,6-cyclohexenyl-(2R,9R)-2,9-diphenyl-14,15-naphtho-4,7-diaza-1,10,13,16-tetraoxaoctadecane

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanol / 72 h / 40 - 60 °C / Inert atmosphere

2.1: sodium hydride / mineral oil; tetrahydrofuran / 2 h / 0 °C / Reflux; Inert atmosphere

2.2: 96 h / 0 °C / Reflux

With sodium hydride; In tetrahydrofuran; methanol; mineral oil;
DOI:10.1016/j.tet.2012.10.020

Reference yield:

: 20780-53-4
(R)-Styrene oxide

: 1415402-93-5
N,N'-Dibenzyl-(5R,6R)-5,6-cyclohexenyl-(2R,9R)-2,9-diphenyl-14,15-naphtho-4,7-diaza-1,10,13,16-tetraoxaoctadecane

Guidance literature:: Multi-step reaction with 2 steps

1.1: methanol / 72 h / 40 - 60 °C / Inert atmosphere

2.1: sodium hydride / mineral oil; tetrahydrofuran / 2 h / 0 °C / Reflux; Inert atmosphere

2.2: 96 h / 0 °C / Reflux

With sodium hydride; In tetrahydrofuran; methanol; mineral oil;
DOI:10.1016/j.tet.2012.10.020